[4-((4,5-bis(methylthio)-1,3-dithiol-2-ylidene)methyl)thienyl-phenyl]dithienylphenylamine

Base Information

Chemical Name:[4-((4,5-bis(methylthio)-1,3-dithiol-2-ylidene)methyl)thienyl-phenyl]dithienylphenylamine
CAS No.:1273594-73-2
Molecular Formula:C₃₆H₂₇NS₇
Molecular Weight:698.079
Hs Code.:

Synonyms:[4-((4,5-bis(methylthio)-1,3-dithiol-2-ylidene)methyl)thienyl-phenyl]dithienylphenylamine

Suppliers and Price of [4-((4,5-bis(methylthio)-1,3-dithiol-2-ylidene)methyl)thienyl-phenyl]dithienylphenylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [4-((4,5-bis(methylthio)-1,3-dithiol-2-ylidene)methyl)thienyl-phenyl]dithienylphenylamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [4-((4,5-bis(methylthio)-1,3-dithiol-2-ylidene)methyl)thienyl-phenyl]dithienylphenylamine

There total 2 articles about [4-((4,5-bis(methylthio)-1,3-dithiol-2-ylidene)methyl)thienyl-phenyl]dithienylphenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 142807-63-4
tris(4-(thiophen-2-yl)phenyl)amine

: 1273594-73-2
[4-((4,5-bis(methylthio)-1,3-dithiol-2-ylidene)methyl)thienyl-phenyl]dithienylphenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / 1,2-dichloro-ethane / Inert atmosphere; Reflux

2: triethyl phosphite / toluene / 4 h / Inert atmosphere; Reflux

With triethyl phosphite; trichlorophosphate; In 1,2-dichloro-ethane; toluene; 1: Vilsmeier formylation;
DOI:10.1039/c0ob00471e

Reference yield:

: 49638-64-4
4,5-bis(methylthio)-1,3-dithiole-2-thione

: 1189743-36-9
[4-(5-formyl-2-thienyl)phenyl]-bis[4-(2-thienyl)phenyl]amine

: 1273594-73-2
[4-((4,5-bis(methylthio)-1,3-dithiol-2-ylidene)methyl)thienyl-phenyl]dithienylphenylamine

Guidance literature:: With triethyl phosphite; In toluene; for 4h; Inert atmosphere; Reflux;
DOI:10.1039/c0ob00471e

Reference yield: 30.0%

: 1273594-73-2
[4-((4,5-bis(methylthio)-1,3-dithiol-2-ylidene)methyl)thienyl-phenyl]dithienylphenylamine

: 1273594-79-8
C₇₂H₅₂N₂S₁₄

Guidance literature:: [4-((4,5-bis(methylthio)-1,3-dithiol-2-ylidene)methyl)thienyl-phenyl]dithienylphenylamine; With hydrogenchloride; tetrafluoroboric acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In diethyl ether; water; at 20 ℃; for 1h;

With zinc; In acetonitrile; at 20 ℃; for 0.75h;
DOI:10.1039/c0ob00471e