methyl 3-{4-[5-(2-acetoxyethyl)-2-methoxyphenoxy]phenyl}-2-hydroxypropionate

Base Information

Chemical Name:methyl 3-{4-[5-(2-acetoxyethyl)-2-methoxyphenoxy]phenyl}-2-hydroxypropionate
CAS No.:945531-01-1
Molecular Formula:C₂₁H₂₄O₇
Molecular Weight:388.417
Hs Code.:

Synonyms:methyl 3-{4-[5-(2-acetoxyethyl)-2-methoxyphenoxy]phenyl}-2-hydroxypropionate

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Chemical Property of methyl 3-{4-[5-(2-acetoxyethyl)-2-methoxyphenoxy]phenyl}-2-hydroxypropionate

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Technology Process of methyl 3-{4-[5-(2-acetoxyethyl)-2-methoxyphenoxy]phenyl}-2-hydroxypropionate

There total 6 articles about methyl 3-{4-[5-(2-acetoxyethyl)-2-methoxyphenoxy]phenyl}-2-hydroxypropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 945531-31-7
C₂₁H₂₂O₇

: 945531-01-1
methyl 3-{4-[5-(2-acetoxyethyl)-2-methoxyphenoxy]phenyl}-2-hydroxypropionate

Guidance literature:: With hydrogen; sodium carbonate; palladium on activated charcoal; In methanol; ethyl acetate; under 2280.15 Torr;
DOI:10.1016/j.tet.2007.03.022

Reference yield:

: C₁₉H₂₀O₆

: 945531-01-1
methyl 3-{4-[5-(2-acetoxyethyl)-2-methoxyphenoxy]phenyl}-2-hydroxypropionate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 18 h / 20 °C

2: 28.7 g / H₂; Na₂CO₃ / Pd/C / ethyl acetate; methanol / 2280.15 Torr

With pyridine; hydrogen; sodium carbonate; palladium on activated charcoal; In methanol; ethyl acetate;
DOI:10.1016/j.tet.2007.03.022

Reference yield:

: 945530-98-3
2-[3-(4-formylphenoxy)-4-methoxyphenyl]ethyl acetate

: 945531-01-1
methyl 3-{4-[5-(2-acetoxyethyl)-2-methoxyphenoxy]phenyl}-2-hydroxypropionate

Guidance literature:: Multi-step reaction with 3 steps

1: 49.7 g / NaOMe / methanol / 18 h / 20 °C

2: pyridine / 18 h / 20 °C

3: 28.7 g / H₂; Na₂CO₃ / Pd/C / ethyl acetate; methanol / 2280.15 Torr

With pyridine; hydrogen; sodium methylate; sodium carbonate; palladium on activated charcoal; In methanol; ethyl acetate;
DOI:10.1016/j.tet.2007.03.022