C₂₉H₃₇FN₂O₅

Base Information

Chemical Name:C₂₉H₃₇FN₂O₅
CAS No.:1352344-90-1
Molecular Formula:C₂₉H₃₇FN₂O₅
Molecular Weight:512.622
Hs Code.:

C<sub>29</sub>H<sub>37</sub>FN<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₉H₃₇FN₂O₅

Suppliers and Price of C₂₉H₃₇FN₂O₅

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of C₂₉H₃₇FN₂O₅

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₉H₃₇FN₂O₅

There total 12 articles about C₂₉H₃₇FN₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 1352344-85-4
C₁₉H₂₆BNO₄

: 1352344-88-7
C₂₃H₃₇FN₂O₄

: C₁₉H₂₈N₂O₃

: 1352344-90-1
C₂₉H₃₇FN₂O₅

: C₂₉H₃₇FN₂O₅

Guidance literature:: C₂₃H₃₇FN₂O₄; With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In diethyl ether; at -78 ℃; Inert atmosphere;

C₁₉H₂₆BNO₄; In diethyl ether; at -98 - -78 ℃; optical yield given as %ee; Further stages; Inert atmosphere;
DOI:10.1016/j.tet.2011.09.142

Reference yield:

: 905710-66-9
4-bromo-3-(hydroxymethyl)benzonitrile

: 1352344-90-1
C₂₉H₃₇FN₂O₅

: C₂₉H₃₇FN₂O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene-4-sulfonic acid / dichloromethane / 15 h / 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran / 0.17 h / -98 °C / Inert atmosphere

2.2: 1.67 h / -98 - 20 °C / Inert atmosphere

3.1: water / tetrahydrofuran / 1 h / 20 °C

4.1: magnesium sulfate / dichloromethane / 15 h / 20 °C / Inert atmosphere

5.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / diethyl ether / -78 °C / Inert atmosphere

5.2: -98 - -78 °C / Inert atmosphere

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; water; sec.-butyllithium; magnesium sulfate; toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.tet.2011.09.142

Reference yield:

: 254744-14-4
2-bromo-5-cyanobenzyl acetate

: 1352344-90-1
C₂₉H₃₇FN₂O₅

: C₂₉H₃₇FN₂O₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: water; sodium hydroxide / methanol / 4 h

2.1: toluene-4-sulfonic acid / dichloromethane / 15 h / 20 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran / 0.17 h / -98 °C / Inert atmosphere

3.2: 1.67 h / -98 - 20 °C / Inert atmosphere

4.1: water / tetrahydrofuran / 1 h / 20 °C

5.1: magnesium sulfate / dichloromethane / 15 h / 20 °C / Inert atmosphere

6.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / diethyl ether / -78 °C / Inert atmosphere

6.2: -98 - -78 °C / Inert atmosphere

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; water; sec.-butyllithium; magnesium sulfate; toluene-4-sulfonic acid; sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1016/j.tet.2011.09.142