7-chloro-3,4-dihydro-10-hydroxy-3-<3-(trifluoromethyl)phenyl>-1,9(2H, 10H)-acridinedione

Base Information

• Chemical Name: 7-chloro-3,4-dihydro-10-hydroxy-3-<3-(trifluoromethyl)phenyl>-1,9(2H, 10H)-acridinedione
• CAS No.: 80061-33-2
• Molecular Formula: C₂₀H₁₃ClF₃NO₃
• Molecular Weight: 407.776

Synonyms:7-chloro-3,4-dihydro-10-hydroxy-3-<3-(trifluoromethyl)phenyl>-1,9(2H, 10H)-acridinedione

Chemical Property of 7-chloro-3,4-dihydro-10-hydroxy-3-<3-(trifluoromethyl)phenyl>-1,9(2H, 10H)-acridinedione

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Technology Process of 7-chloro-3,4-dihydro-10-hydroxy-3-<3-(trifluoromethyl)phenyl>-1,9(2H, 10H)-acridinedione

There total 1 articles about 7-chloro-3,4-dihydro-10-hydroxy-3-<3-(trifluoromethyl)phenyl>-1,9(2H, 10H)-acridinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

5-(3-Trifluoromethyl-phenyl)-cyclohexane-1,3-dione (144128-67-6) + 2-nitro-benzaldehyde (552-89-6) → 7-chloro-3,4-dihydro-10-hydroxy-3-<3-(trifluoromethyl)phenyl>-1,9(2H, 10H)-acridinedione (80061-33-2)

Guidance literature:

With hydrogenchloride; acetic acid; at 85 ℃; for 4h;

DOI:10.1021/jm00097a001

Reference yield: 100.0%

7-chloro-3,4-dihydro-10-hydroxy-3-<3-(trifluoromethyl)phenyl>-1,9(2H, 10H)-acridinedione (80061-33-2) + N2-Butyl-butane-1,2-diamine (80092-87-1) → 1-[(E)-2-Butylamino-butylimino]-7-chloro-10-hydroxy-3-(3-trifluoromethyl-phenyl)-1,3,4,10-tetrahydro-2H-acridin-9-one (80092-46-2)

Guidance literature:

In ethanol; for 1.5h; Heating;

DOI:10.1021/jm00097a001

Reference yield: 95.0%

5-(pyrrolidin-1-yl)pentan-1-amine (71302-71-1) + 7-chloro-3,4-dihydro-10-hydroxy-3-<3-(trifluoromethyl)phenyl>-1,9(2H, 10H)-acridinedione (80061-33-2) → 7-Chloro-10-hydroxy-1-[(E)-5-pyrrolidin-1-yl-pentylimino]-3-(3-trifluoromethyl-phenyl)-1,3,4,10-tetrahydro-2H-acridin-9-one (144128-48-3)

Guidance literature:

In ethanol; for 1.5h; Heating;

DOI:10.1021/jm00097a001

upstream raw materials:

5-(3-Trifluoromethyl-phenyl)-cyclohexane-1,3-dione

2-nitro-benzaldehyde

Downstream raw materials:

7-Chloro-1,3,4,10-tetrahydro-10-hydroxy-1-[[2-[1-pyrrolidinyl]ethyl]imino]-3-[3-(trifluoromethyl)phenyl]-9(2H)-acridinone

7-Chloro-10-hydroxy-1-[(E)-4-pyrrolidin-1-yl-butylimino]-3-(3-trifluoromethyl-phenyl)-1,3,4,10-tetrahydro-2H-acridin-9-one

7-Chloro-10-hydroxy-1-[(E)-5-pyrrolidin-1-yl-pentylimino]-3-(3-trifluoromethyl-phenyl)-1,3,4,10-tetrahydro-2H-acridin-9-one

7-Chloro-10-hydroxy-1-[(E)-3-pyrrolidin-1-yl-propylimino]-3-(3-trifluoromethyl-phenyl)-1,3,4,10-tetrahydro-2H-acridin-9-one

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