7-Benzyloxy-1-<2-(2-methyl-1,3-dioxolan-2-yl)benzyl>-6-methoxyisochinolin

Base Information

• Chemical Name: 7-Benzyloxy-1-<2-(2-methyl-1,3-dioxolan-2-yl)benzyl>-6-methoxyisochinolin
• CAS No.: 150982-75-5
• Molecular Formula: C₂₈H₂₇NO₄
• Molecular Weight: 441.527

Synonyms:7-Benzyloxy-1-<2-(2-methyl-1,3-dioxolan-2-yl)benzyl>-6-methoxyisochinolin

Chemical Property of 7-Benzyloxy-1-<2-(2-methyl-1,3-dioxolan-2-yl)benzyl>-6-methoxyisochinolin

Chemical Property:

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Technology Process of 7-Benzyloxy-1-<2-(2-methyl-1,3-dioxolan-2-yl)benzyl>-6-methoxyisochinolin

There total 2 articles about 7-Benzyloxy-1-<2-(2-methyl-1,3-dioxolan-2-yl)benzyl>-6-methoxyisochinolin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-Benzoyl-7-benzyloxy-1-<2-(2-methyl-1,3-dioxolan-2-yl)benzyl>-1-cyan-6-methoxy-1,2-dihydroisochinolin (150982-73-3) → 7-Benzyloxy-1-<2-(2-methyl-1,3-dioxolan-2-yl)benzyl>-6-methoxyisochinolin (150982-75-5)

Guidance literature:

With potassium hydroxide; In methanol; for 0.333333h; Heating;

DOI:10.1002/ardp.19933260502

Reference yield:

2-benzoyl-7-benzyloxy-1,2-dihydro-6-methoxyisoquinoline-1-carbonitrile (107588-82-9) → 7-Benzyloxy-1-<2-(2-methyl-1,3-dioxolan-2-yl)benzyl>-6-methoxyisochinolin (150982-75-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 63 percent / KOH, KI / CH₂Cl₂ / 26 h / Ambient temperature

2: 95 percent / aq. KOH / methanol / 0.33 h / Heating

With potassium hydroxide; potassium iodide; In methanol; dichloromethane;

DOI:10.1002/ardp.19933260502

Reference yield: 98.0%

7-Benzyloxy-1-<2-(2-methyl-1,3-dioxolan-2-yl)benzyl>-6-methoxyisochinolin (150982-75-5) → 2-Benzyloxy-3-methoxy-8-methyl-dibenzochinolizinium-chlorid

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; for 3h; Ambient temperature;

DOI:10.1002/ardp.19933260502

upstream raw materials:

2-Benzoyl-7-benzyloxy-1-<2-(2-methyl-1,3-dioxolan-2-yl)benzyl>-1-cyan-6-methoxy-1,2-dihydroisochinolin

2-benzoyl-7-benzyloxy-1,2-dihydro-6-methoxyisoquinoline-1-carbonitrile

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