N-{8-[(5,11-bis(2-nitrobenzenesulfonyl)-1-oxa-5,11-diazacyclotetradecanyl)-1,4-phenylenebis(methylene)]}-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine

Base Information

• Chemical Name: N-{8-[(5,11-bis(2-nitrobenzenesulfonyl)-1-oxa-5,11-diazacyclotetradecanyl)-1,4-phenylenebis(methylene)]}-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine
• CAS No.: 344950-57-8
• Molecular Formula: C₄₃H₄₇N₇O₁₃S₃
• Molecular Weight: 966.083

Synonyms:N-{8-[(5,11-bis(2-nitrobenzenesulfonyl)-1-oxa-5,11-diazacyclotetradecanyl)-1,4-phenylenebis(methylene)]}-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine

Chemical Property of N-{8-[(5,11-bis(2-nitrobenzenesulfonyl)-1-oxa-5,11-diazacyclotetradecanyl)-1,4-phenylenebis(methylene)]}-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine

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Technology Process of N-{8-[(5,11-bis(2-nitrobenzenesulfonyl)-1-oxa-5,11-diazacyclotetradecanyl)-1,4-phenylenebis(methylene)]}-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine

There total 1 articles about N-{8-[(5,11-bis(2-nitrobenzenesulfonyl)-1-oxa-5,11-diazacyclotetradecanyl)-1,4-phenylenebis(methylene)]}-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

N,N'-bis(2-nitrobenzenesulfonyl)-bis(3-aminopropyl) ether (344950-59-0) + methanesulfonic acid 5-methanesulfonyloxy-3-(4-{[(2-nitrobenzenesulfonyl)pyridin-2-ylmethyl-amino]methyl}benzyl)pentyl ester (344950-52-3) → N-{8-[(5,11-bis(2-nitrobenzenesulfonyl)-1-oxa-5,11-diazacyclotetradecanyl)-1,4-phenylenebis(methylene)]}-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine (344950-57-8)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 40h; Inert atmosphere;

DOI:10.1021/jm901530b

Reference yield: 57.0%

N-{8-[(5,11-bis(2-nitrobenzenesulfonyl)-1-oxa-5,11-diazacyclotetradecanyl)-1,4-phenylenebis(methylene)]}-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine (344950-57-8) → N-(12-(5-oxa-1,9-diazacyclotetradecanyl-1,4-phenylenebis(methylene))-2-(aminomethyl)pyridine (344950-26-1)

Guidance literature:

With potassium carbonate; thiophenol; In acetonitrile; at 20 ℃;

DOI:10.1021/jm901530b

upstream raw materials:

N,N'-bis(2-nitrobenzenesulfonyl)-bis(3-aminopropyl) ether

methanesulfonic acid 5-methanesulfonyloxy-3-(4-{[(2-nitrobenzenesulfonyl)pyridin-2-ylmethyl-amino]methyl}benzyl)pentyl ester

Downstream raw materials:

N-(12-(5-oxa-1,9-diazacyclotetradecanyl-1,4-phenylenebis(methylene))-2-(aminomethyl)pyridine

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