Technology Process of C41H62N6O7Si
There total 8 articles about C41H62N6O7Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C16H28BNO5Si; C25H36IN5O4;
With
potassium acetate; caesium carbonate;
In
dimethyl sulfoxide;
for 0.166667h;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
dimethyl sulfoxide;
at 70 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation
1.2: 1 h
2.1: pyridine hydrogenfluoride / tetrahydrofuran / 3 h / 20 °C
3.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 2 h / 0 °C
3.2: 2 h
3.3: 5 h
4.1: potassium acetate; caesium carbonate / dimethyl sulfoxide / 0.17 h
4.2: 1 h / 70 °C
With
titanium(IV) isopropylate; potassium acetate; diisobutylaluminium hydride; caesium carbonate; pyridine hydrogenfluoride;
In
tetrahydrofuran; dimethyl sulfoxide; toluene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 16 h / pH 2
1.2: pH 7 / Alkaline aqueous solution
2.1: benzene / Heating / reflux
3.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation
3.2: 1 h
4.1: pyridine hydrogenfluoride / tetrahydrofuran / 3 h / 20 °C
5.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 2 h / 0 °C
5.2: 2 h
5.3: 5 h
6.1: potassium acetate; caesium carbonate / dimethyl sulfoxide / 0.17 h
6.2: 1 h / 70 °C
With
titanium(IV) isopropylate; hydrogenchloride; methyl orange; potassium acetate; diisobutylaluminium hydride; sodium cyanoborohydride; caesium carbonate; pyridine hydrogenfluoride;
In
tetrahydrofuran; methanol; water; dimethyl sulfoxide; toluene; benzene;
