3,3'-bis(2-hydroxybenzaldehyde)

Base Information

Chemical Name:3,3'-bis(2-hydroxybenzaldehyde)
CAS No.:121073-78-7
Molecular Formula:C₁₈H₁₈O₇
Molecular Weight:346.337
Hs Code.:

3,3'-<Oxybis(2,1-ethanediyloxy)>bis(2-hydroxybenzaldehyde)

Synonyms:3,3'-bis(2-hydroxybenzaldehyde)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,3'-bis(2-hydroxybenzaldehyde)

Chemical Property:

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Technology Process of 3,3'-bis(2-hydroxybenzaldehyde)

There total 1 articles about 3,3'-bis(2-hydroxybenzaldehyde) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 24677-78-9
2,3-dihydroxybenzaldehyde

: 7460-82-4
diethylene glycol ditosylate

: 121073-78-7
3,3'-bis(2-hydroxybenzaldehyde)

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; for 20h; Ambient temperature;
DOI:10.1021/jo00001a043

Reference yield: 89.5%

: N,N-bis(2-aminoethyl)-2-hydroxybenzylamine trishydrochloride

: lutetium(III) acetate hydrate

: 121073-78-7
3,3'-bis(2-hydroxybenzaldehyde)

: 67-63-0,8013-70-5
isopropyl alcohol

: 1310-73-2
sodium hydroxide

: C₂₉H₃₄N₃O₆^(3-)*Lu⁽³⁺⁾*Na⁽¹⁺⁾*2C₃H₈O*C₂H₃O₂^(1-)

Guidance literature:: N,N-bis(2-aminoethyl)-2-hydroxybenzylamine trishydrochloride; lutetium(III) acetate hydrate; 3,3'-bis(2-hydroxybenzaldehyde); sodium hydroxide; In methanol; for 1h; Reflux;

With sodium tetrahydroborate; In methanol; for 1h; Reflux;

isopropyl alcohol;
DOI:10.1016/j.ica.2014.03.032