ethyl (E)-4-<2-(3,4-dihydro-4,4-dimethyl-2H-1-benzopyran-6-yl)-2-propenal>benzoate

Base Information

Chemical Name:ethyl (E)-4-<2-(3,4-dihydro-4,4-dimethyl-2H-1-benzopyran-6-yl)-2-propenal>benzoate
CAS No.:150799-39-6
Molecular Formula:C₂₃H₂₄O₄
Molecular Weight:364.441
Hs Code.:

Synonyms:ethyl (E)-4-<2-(3,4-dihydro-4,4-dimethyl-2H-1-benzopyran-6-yl)-2-propenal>benzoate

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Chemical Property of ethyl (E)-4-<2-(3,4-dihydro-4,4-dimethyl-2H-1-benzopyran-6-yl)-2-propenal>benzoate

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Technology Process of ethyl (E)-4-<2-(3,4-dihydro-4,4-dimethyl-2H-1-benzopyran-6-yl)-2-propenal>benzoate

There total 2 articles about ethyl (E)-4-<2-(3,4-dihydro-4,4-dimethyl-2H-1-benzopyran-6-yl)-2-propenal>benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 150799-37-4
ethyl (E)-4-<2-(3,4-dihydro-4,4-dimethyl-2H-1-benzopyran-6-yl)-3-hydroxy-1-propenyl>benzoate

: 150799-39-6
ethyl (E)-4-<2-(3,4-dihydro-4,4-dimethyl-2H-1-benzopyran-6-yl)-2-propenal>benzoate

Guidance literature:: With manganese(IV) oxide; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1002/jps.2600820522

Reference yield:

: 88579-28-6
ethyl p-[(E)-2-(4,4-dimethyl-6-chromanyl)propenyl]-benzoate

: 150799-39-6
ethyl (E)-4-<2-(3,4-dihydro-4,4-dimethyl-2H-1-benzopyran-6-yl)-2-propenal>benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 31.2 percent / SeO₂ / aq. ethanol / 24 h / Heating

2: 76 percent / MnO₂ / CH₂Cl₂ / 24 h / Ambient temperature

With manganese(IV) oxide; selenium(IV) oxide; In ethanol; dichloromethane;
DOI:10.1002/jps.2600820522

Reference yield: 82.0%

: 150799-39-6
ethyl (E)-4-<2-(3,4-dihydro-4,4-dimethyl-2H-1-benzopyran-6-yl)-2-propenal>benzoate

: ethyl (E)-4-<2-(3,4-dihydro-4,4-dimethyl-2H-1-benzopyran-6-yl)-2-propenoic acid>benzoate

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; recorcinol; In water; tert-butyl alcohol; for 24h; Ambient temperature;
DOI:10.1002/jps.2600820522