C₅₈H₆₄N₁₃O₁₂PS₆

Base Information

• Chemical Name: C₅₈H₆₄N₁₃O₁₂PS₆
• CAS No.: 960062-83-3
• Molecular Formula: C₅₈H₆₄N₁₃O₁₂PS₆
• Molecular Weight: 1358.6
• Mol file: 960062-83-3.mol

Synonyms:C₅₈H₆₄N₁₃O₁₂PS₆

Chemical Property of C₅₈H₆₄N₁₃O₁₂PS₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₈H₆₄N₁₃O₁₂PS₆

There total 7 articles about C₅₈H₆₄N₁₃O₁₂PS₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

GE2270 A → C58H64N13O12PS6 (960062-83-3)

Guidance literature:

Multi-step reaction with 7 steps

1.1: water; sodium hydroxide / tetrahydrofuran / 1.5 h / 60 °C

2.1: chloroformic acid ethyl ester; triethylamine / acetone / 1 h

2.2: 1.33 h / 60 °C

3.1: 2 h / 80 °C

4.1: pyridine; dmap / 3 h

5.1: dichloromethane / 0.5 h

6.1: water; sodium hydrogencarbonate / ethyl acetate

7.1: pyridine

With pyridine; dmap; water; chloroformic acid ethyl ester; sodium hydrogencarbonate; triethylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; ethyl acetate; acetone;

DOI:10.1021/jm200938f

Reference yield:

C54H55N13O10S6 (960061-71-6) → C58H64N13O12PS6 (960062-83-3)

Guidance literature:

Multi-step reaction with 3 steps

1: dichloromethane / 0.5 h

2: water; sodium hydrogencarbonate / ethyl acetate

3: pyridine

With pyridine; water; sodium hydrogencarbonate; In dichloromethane; ethyl acetate;

DOI:10.1021/jm200938f

Reference yield:

C48H43N15O8S6 (960061-69-2) → C58H64N13O12PS6 (960062-83-3)

Guidance literature:

Multi-step reaction with 5 steps

1: 2 h / 80 °C

2: pyridine; dmap / 3 h

3: dichloromethane / 0.5 h

4: water; sodium hydrogencarbonate / ethyl acetate

5: pyridine

With pyridine; dmap; water; sodium hydrogencarbonate; In dichloromethane; ethyl acetate;

DOI:10.1021/jm200938f

upstream raw materials:

C₅₄H₅₅N₁₃O₁₀S₆

C₄₈H₄₃N₁₅O₈S₆

C₄₈H₄₄N₁₂O₉S₆

C₅₂H₅₃N₁₃O₉S₆

Downstream raw materials:

C₅₄H₅₆N₁₃O₁₂PS₆

C₅₂H₅₄N₁₃O₁₁PS₆

Refernces