Technology Process of C29H37NO5Si
There total 6 articles about C29H37NO5Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
4-ethynylveratrole;
With
n-butyllithium;
In
tetrahydrofuran; hexanes;
at -78 ℃;
for 0.25h;
Inert atmosphere;
CF3O3S(1-)*C19H28NO3Si(1+);
In
tetrahydrofuran; hexanes;
at -90 ℃;
for 0.333333h;
Inert atmosphere;
DOI:10.1002/anie.201102226
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tetrahydrofuran / 0.5 h / -78 - -60 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran; hexanes / 0.25 h / -78 °C / Inert atmosphere
2.2: 0.33 h / -90 °C / Inert atmosphere
With
n-butyllithium;
In
tetrahydrofuran; hexanes;
DOI:10.1002/anie.201102226
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: formic acid; dihydrogen peroxide / water / 5 h / 0 °C / Inert atmosphere
2.1: trifluorormethanesulfonic acid; (S)-3,3-diphenyl-1-(o-tolyl)hexahydropyrrolo[1,2-c]-[1,3,2]oxazaborole / dichloromethane; toluene / 2 h / -78 °C / Inert atmosphere
3.1: trimethylphosphane / diethyl ether / 1 h / 0 - 24 °C / Inert atmosphere
4.1: tetrahydrofuran / 0.5 h / -78 - -60 °C / Inert atmosphere
5.1: n-butyllithium / tetrahydrofuran; hexanes / 0.25 h / -78 °C / Inert atmosphere
5.2: 0.33 h / -90 °C / Inert atmosphere
With
n-butyllithium; formic acid; trifluorormethanesulfonic acid; dihydrogen peroxide; (S)-3,3-diphenyl-1-(o-tolyl)hexahydropyrrolo[1,2-c]-[1,3,2]oxazaborole; trimethylphosphane;
In
tetrahydrofuran; hexanes; diethyl ether; dichloromethane; water; toluene;
2.1: Diels-Alder reaction / 3.1: Staudinger reaction;
DOI:10.1002/anie.201102226
