(2,4-difluorophenyl){(E)-2-phenylethenyl}iodonium trifluoromethanesulfonate

Base Information

Chemical Name:(2,4-difluorophenyl){(E)-2-phenylethenyl}iodonium trifluoromethanesulfonate
CAS No.:1428541-16-5
Molecular Formula:C₁₅H₁₀F₅IO₃S
Molecular Weight:492.205
Hs Code.:

Synonyms:(2,4-difluorophenyl){(E)-2-phenylethenyl}iodonium trifluoromethanesulfonate

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Chemical Property of (2,4-difluorophenyl){(E)-2-phenylethenyl}iodonium trifluoromethanesulfonate

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Technology Process of (2,4-difluorophenyl){(E)-2-phenylethenyl}iodonium trifluoromethanesulfonate

There total 2 articles about (2,4-difluorophenyl){(E)-2-phenylethenyl}iodonium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1493-13-6
trifluorormethanesulfonic acid

: 6783-05-7
trans-2-phenylvinylboronic acid

: 1428541-13-2
bis(acetyloxy)(2,4-difluorophenyl)-λ³-iodane

: 1428541-16-5
(2,4-difluorophenyl){(E)-2-phenylethenyl}iodonium trifluoromethanesulfonate

Guidance literature:: trans-2-phenylvinylboronic acid; With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 0.25h; Inert atmosphere;

bis(acetyloxy)(2,4-difluorophenyl)-λ³-iodane; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;

trifluorormethanesulfonic acid; In dichloromethane; at 0 ℃; for 0.25h;
DOI:10.1021/ja401840j

Reference yield:

: 2265-93-2
2,4-difluoro-1-iodobenzene

: 1428541-16-5
(2,4-difluorophenyl){(E)-2-phenylethenyl}iodonium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium peroxoborate tetrahydrate / 0.33 h / 45 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: boron trifluoride diethyl etherate / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

2.2: 1 h / 0 °C / Inert atmosphere

2.3: 0.25 h / 0 °C

With sodium peroxoborate tetrahydrate; boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1021/ja401840j