(Z)-2-[(4-methylthiosemicarbazono)-(4-nitrophenyl)methyl]-4,5-methylenedioxytoluene

Base Information

Chemical Name:(Z)-2-[(4-methylthiosemicarbazono)-(4-nitrophenyl)methyl]-4,5-methylenedioxytoluene
CAS No.:741261-88-1
Molecular Formula:C₁₇H₁₆N₄O₄S
Molecular Weight:372.404
Hs Code.:

Synonyms:(Z)-2-[(4-methylthiosemicarbazono)-(4-nitrophenyl)methyl]-4,5-methylenedioxytoluene

Suppliers and Price of (Z)-2-[(4-methylthiosemicarbazono)-(4-nitrophenyl)methyl]-4,5-methylenedioxytoluene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (Z)-2-[(4-methylthiosemicarbazono)-(4-nitrophenyl)methyl]-4,5-methylenedioxytoluene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (Z)-2-[(4-methylthiosemicarbazono)-(4-nitrophenyl)methyl]-4,5-methylenedioxytoluene

There total 1 articles about (Z)-2-[(4-methylthiosemicarbazono)-(4-nitrophenyl)methyl]-4,5-methylenedioxytoluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 6610-29-3
4-methylthiosemicarbazide

: 295793-35-0
(6-methyl-1,3-benzodioxol-5-yl)-(4-nitrophenyl)-methanone

: 741261-88-1
(Z)-2-[(4-methylthiosemicarbazono)-(4-nitrophenyl)methyl]-4,5-methylenedioxytoluene

Guidance literature:: With hydrogenchloride; In methanol; for 48h; Heating;
DOI:10.1016/j.bmc.2004.04.015

Reference yield: 80.0%

: 741261-88-1
(Z)-2-[(4-methylthiosemicarbazono)-(4-nitrophenyl)methyl]-4,5-methylenedioxytoluene

: 741261-93-8
(Z)-2-[(4-aminophenyl)-(4-methylthiosemicarbazono)-methyl]-4,5-methylenedioxytoluene

Guidance literature:: With ammonium formate; nickel; In ethanol; for 2h; Heating;
DOI:10.1016/j.bmc.2004.04.015

Reference yield:

: 741261-88-1
(Z)-2-[(4-methylthiosemicarbazono)-(4-nitrophenyl)methyl]-4,5-methylenedioxytoluene

: (Z)-2-[(4-aminophenyl)-(4-methylsemicarbazono)-methyl]-4,5-methylenedioxytoluene

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / ammonium formate; Raney-Ni / ethanol / 2 h / Heating

2: 83 percent / H₂O₂; NaOMe / methanol / 20 °C

With dihydrogen peroxide; sodium methylate; ammonium formate; nickel; In methanol; ethanol;
DOI:10.1016/j.bmc.2004.04.015