4-azido-3-O-<2'-azido-6'-(benzyloxycarbonylamino)-2',3',4',6'-tetradeoxy-α-D-threo-hexopyranosyl>-1,4,5-trideoxy-6-O-methyl-1-(benzyloxycarbonyl-glycyl)-methylamino-D-chiro-inositol

Base Information

Chemical Name:4-azido-3-O-<2'-azido-6'-(benzyloxycarbonylamino)-2',3',4',6'-tetradeoxy-α-D-threo-hexopyranosyl>-1,4,5-trideoxy-6-O-methyl-1-(benzyloxycarbonyl-glycyl)-methylamino-D-chiro-inositol
CAS No.:169103-91-7
Molecular Formula:C₃₂H₄₁N₉O₉
Molecular Weight:695.732
Hs Code.:

4-azido-3-O-<2'-azido-6'-(benzyloxycarbonylamino)-2',3',4',6'-tetradeoxy-α-D-threo-hexopyranosyl>-1,4,5-trideoxy-6-O-methyl-1-(benzyloxycarbonyl-glycyl)-methylamino-D-chiro-inositol

Synonyms:4-azido-3-O-<2'-azido-6'-(benzyloxycarbonylamino)-2',3',4',6'-tetradeoxy-α-D-threo-hexopyranosyl>-1,4,5-trideoxy-6-O-methyl-1-(benzyloxycarbonyl-glycyl)-methylamino-D-chiro-inositol

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Chemical Property of 4-azido-3-O-<2'-azido-6'-(benzyloxycarbonylamino)-2',3',4',6'-tetradeoxy-α-D-threo-hexopyranosyl>-1,4,5-trideoxy-6-O-methyl-1-(benzyloxycarbonyl-glycyl)-methylamino-D-chiro-inositol

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Technology Process of 4-azido-3-O-<2'-azido-6'-(benzyloxycarbonylamino)-2',3',4',6'-tetradeoxy-α-D-threo-hexopyranosyl>-1,4,5-trideoxy-6-O-methyl-1-(benzyloxycarbonyl-glycyl)-methylamino-D-chiro-inositol

There total 6 articles about 4-azido-3-O-<2'-azido-6'-(benzyloxycarbonylamino)-2',3',4',6'-tetradeoxy-α-D-threo-hexopyranosyl>-1,4,5-trideoxy-6-O-methyl-1-(benzyloxycarbonyl-glycyl)-methylamino-D-chiro-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 2899-60-7
Cbz-Gly-ONSuc

: 169103-90-6
4-azido-3-O-<2'-azido-6'-(benzyloxycarbonylamino)-2',3',4',6'-tetradeoxy-α-D-threo-hexopyranosyl>-1,4,5-trideoxy-6-O-methyl-1-methylamino-D-chiro-inositol

: 169103-91-7
4-azido-3-O-<2'-azido-6'-(benzyloxycarbonylamino)-2',3',4',6'-tetradeoxy-α-D-threo-hexopyranosyl>-1,4,5-trideoxy-6-O-methyl-1-(benzyloxycarbonyl-glycyl)-methylamino-D-chiro-inositol

Guidance literature:: In N,N-dimethyl-formamide; at 70 ℃; for 7h;

Reference yield:

: Acetic acid (3S,6S)-3-azido-6-[(2,4-dinitro-phenylamino)-methyl]-tetrahydro-pyran-2-yl ester

: 169103-91-7
4-azido-3-O-<2'-azido-6'-(benzyloxycarbonylamino)-2',3',4',6'-tetradeoxy-α-D-threo-hexopyranosyl>-1,4,5-trideoxy-6-O-methyl-1-(benzyloxycarbonyl-glycyl)-methylamino-D-chiro-inositol

Guidance literature:: Multi-step reaction with 5 steps

1: 64 percent Turnov_. / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 1 h / Ambient temperature

2: 74 percent / Ba(OH)2*8H₂O / dioxane; H₂O / 26 h / Heating

3: 61 percent / dimethylformamide / 4 h / Ambient temperature

4: 72 percent / Ba(OH)2*8H₂O / dioxane; H₂O / 4 h / 80 °C

5: 63 percent / dimethylformamide / 7 h / 70 °C

With barium dihydroxide; trimethylsilyl trifluoromethanesulfonate; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 169103-79-1
4-azido-3-O-<2'-azido-2',3',4',6'-tetradeoxy-6'-(2,4-dinitrophenylamino)-α-D-threo-hexopyranosyl>-1-N,2-O-carbonyl-1,4,5-trideoxy-6-O-methyl-1-(methylamino)-D-chiro-inositol

: 169103-91-7
4-azido-3-O-<2'-azido-6'-(benzyloxycarbonylamino)-2',3',4',6'-tetradeoxy-α-D-threo-hexopyranosyl>-1,4,5-trideoxy-6-O-methyl-1-(benzyloxycarbonyl-glycyl)-methylamino-D-chiro-inositol

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / Ba(OH)2*8H₂O / dioxane; H₂O / 26 h / Heating

2: 61 percent / dimethylformamide / 4 h / Ambient temperature

3: 72 percent / Ba(OH)2*8H₂O / dioxane; H₂O / 4 h / 80 °C

4: 63 percent / dimethylformamide / 7 h / 70 °C

With barium dihydroxide; In 1,4-dioxane; water; N,N-dimethyl-formamide;