(2R,3S,5R)-2-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-perylen-3-yl-tetrahydro-furan-3-ol

Base Information

Chemical Name:(2R,3S,5R)-2-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-perylen-3-yl-tetrahydro-furan-3-ol
CAS No.:830346-91-3
Molecular Formula:C₄₆H₃₈O₅
Molecular Weight:670.805
Hs Code.:

Synonyms:(2R,3S,5R)-2-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-perylen-3-yl-tetrahydro-furan-3-ol

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Chemical Property of (2R,3S,5R)-2-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-perylen-3-yl-tetrahydro-furan-3-ol

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Technology Process of (2R,3S,5R)-2-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-perylen-3-yl-tetrahydro-furan-3-ol

There total 3 articles about (2R,3S,5R)-2-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-perylen-3-yl-tetrahydro-furan-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 830346-88-8
(2R,3S,5R)-2-Hydroxymethyl-5-perylen-3-yl-tetrahydro-furan-3-ol

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 830346-91-3
(2R,3S,5R)-2-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-perylen-3-yl-tetrahydro-furan-3-ol

Guidance literature:: With pyridine; for 21h;
DOI:10.1039/b410695d

Reference yield:

: 198-55-0
PERYLENE

: 830346-91-3
(2R,3S,5R)-2-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-perylen-3-yl-tetrahydro-furan-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 190 mg / SnCl₄ / 1,2-dichloro-ethane / 3 h / 20 °C

2: 86 percent / NaOMe / methanol; CH₂Cl₂ / 15 h

3: 82 percent / pyridine / 21 h

With pyridine; sodium methylate; tin(IV) chloride; In methanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1039/b410695d

Reference yield:

: 830346-85-5
C₄₁H₃₂O₅

: 830346-91-3
(2R,3S,5R)-2-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-perylen-3-yl-tetrahydro-furan-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / NaOMe / methanol; CH₂Cl₂ / 15 h

2: 82 percent / pyridine / 21 h

With pyridine; sodium methylate; In methanol; dichloromethane;
DOI:10.1039/b410695d