N-(bicyclo[2.2.1]heptan-2-yl)-3,5-bis(trifluoromethyl)-N'-methylbenzohydrazide

Base Information

Chemical Name:N-(bicyclo[2.2.1]heptan-2-yl)-3,5-bis(trifluoromethyl)-N'-methylbenzohydrazide
CAS No.:1263000-64-1
Molecular Formula:C₁₇H₁₈F₆N₂O
Molecular Weight:380.333
Hs Code.:

Synonyms:N-(bicyclo[2.2.1]heptan-2-yl)-3,5-bis(trifluoromethyl)-N'-methylbenzohydrazide

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Chemical Property of N-(bicyclo[2.2.1]heptan-2-yl)-3,5-bis(trifluoromethyl)-N'-methylbenzohydrazide

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Technology Process of N-(bicyclo[2.2.1]heptan-2-yl)-3,5-bis(trifluoromethyl)-N'-methylbenzohydrazide

There total 5 articles about N-(bicyclo[2.2.1]heptan-2-yl)-3,5-bis(trifluoromethyl)-N'-methylbenzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 498-66-8
norborn-2-ene

: 1263000-53-8
3,5-bis(trifluoromethyl)-N'-methylbenzohydrazide

: 1263000-64-1
N-(bicyclo[2.2.1]heptan-2-yl)-3,5-bis(trifluoromethyl)-N'-methylbenzohydrazide

: 1263000-66-3
N'-(bicyclo-[2.2.1]heptan-2-yl)-3,5-bis(trifluoromethyl)-N'-methylbenzohydrazide

Guidance literature:: In α,α,α-trifluorotoluene; at 160 ℃; for 18h; Inert atmosphere;
DOI:10.1039/c0cc02403a

Reference yield:

: 1232355-08-6
C₁₆H₁₀F₆N₂O

: 1263000-64-1
N-(bicyclo[2.2.1]heptan-2-yl)-3,5-bis(trifluoromethyl)-N'-methylbenzohydrazide

: 1263000-66-3
N'-(bicyclo-[2.2.1]heptan-2-yl)-3,5-bis(trifluoromethyl)-N'-methylbenzohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride; sodium cyanoborohydride / tert-butyl alcohol / 30 °C / Inert atmosphere

2: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.08 h / 0 °C

3: 10% palladium on activated carbon; hydrogen / ethyl acetate

4: α,α,α-trifluorotoluene / 18 h / 160 °C / Inert atmosphere

With hydrogenchloride; 10% palladium on activated carbon; hydrogen; sodium hydride; sodium cyanoborohydride; In tetrahydrofuran; α,α,α-trifluorotoluene; ethyl acetate; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1039/c0cc02403a

Reference yield:

: N'-benzyl-N'-methyl-3,5-bis(trifluoromethyl)benzohydrazide

: 1263000-64-1
N-(bicyclo[2.2.1]heptan-2-yl)-3,5-bis(trifluoromethyl)-N'-methylbenzohydrazide

: 1263000-66-3
N'-(bicyclo-[2.2.1]heptan-2-yl)-3,5-bis(trifluoromethyl)-N'-methylbenzohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 10% palladium on activated carbon; hydrogen / ethyl acetate

2: α,α,α-trifluorotoluene / 18 h / 160 °C / Inert atmosphere

With 10% palladium on activated carbon; hydrogen; In α,α,α-trifluorotoluene; ethyl acetate;
DOI:10.1039/c0cc02403a