C₁₄H₁₂⁽²⁾HNO₂S

Base Information

Chemical Name:C₁₄H₁₂⁽²⁾HNO₂S
CAS No.:1309368-27-1
Molecular Formula:C₁₄H₁₃NO₂S
Molecular Weight:260.321
Hs Code.:

C<sub>14</sub>H<sub>12</sub><sup>(2)</sup>HNO<sub>2</sub>S

Synonyms:C₁₄H₁₂⁽²⁾HNO₂S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₂⁽²⁾HNO₂S

Chemical Property:

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Technology Process of C₁₄H₁₂⁽²⁾HNO₂S

There total 5 articles about C₁₄H₁₂⁽²⁾HNO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-phenyl-2H-1λ⁶-benzo[e][1,2]thiazine 1,1-dioxide

: 1309368-27-1
C₁₄H₁₂⁽²⁾HNO₂S

Guidance literature:: With palladium(II) trifluoroacetate; 2,2,2-trifluoroethanol-d₁; (R,S)-JosiPhos; hydrogen; In 2,2,2-trifluoroethanol; at 60 ℃; for 18h; under 7600.51 Torr; Autoclave;
DOI:10.1039/c1cc10313j

Reference yield:

: 960319-19-1
N-Boc-2-(2-hydroxy-2-phenylethyl)benzenesulfonamide

: 1309368-27-1
C₁₄H₁₂⁽²⁾HNO₂S

Guidance literature:: Multi-step reaction with 3 steps

1: pyridinium chlorochromate / dichloromethane / 20 °C

2: trifluoroacetic acid / dichloromethane / Reflux

3: palladium(II) trifluoroacetate; (R,S)-JosiPhos; 2,2,2-trifluoroethanol-d₁; hydrogen / 2,2,2-trifluoroethanol / 18 h / 60 °C / 7600.51 Torr / Autoclave

With palladium(II) trifluoroacetate; 2,2,2-trifluoroethanol-d₁; (R,S)-JosiPhos; hydrogen; pyridinium chlorochromate; trifluoroacetic acid; In dichloromethane; 2,2,2-trifluoroethanol;
DOI:10.1039/c1cc10313j

Reference yield:

: 1309367-79-0
2-(o-tert-butyl phenylsulfonylcarbamate)-1-phenylethanone

: 1309368-27-1
C₁₄H₁₂⁽²⁾HNO₂S

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / Reflux

2: palladium(II) trifluoroacetate; (R,S)-JosiPhos; 2,2,2-trifluoroethanol-d₁; hydrogen / 2,2,2-trifluoroethanol / 18 h / 60 °C / 7600.51 Torr / Autoclave

With palladium(II) trifluoroacetate; 2,2,2-trifluoroethanol-d₁; (R,S)-JosiPhos; hydrogen; trifluoroacetic acid; In dichloromethane; 2,2,2-trifluoroethanol;
DOI:10.1039/c1cc10313j