N-{1-[8-(2-chlorophenyl)-9-(4-chlorophenyl)-9H-purin-6-yl]piperidin-4-yl}-1,1,1-trifluoromethanesulfonamide

Base Information

Chemical Name:N-{1-[8-(2-chlorophenyl)-9-(4-chlorophenyl)-9H-purin-6-yl]piperidin-4-yl}-1,1,1-trifluoromethanesulfonamide
CAS No.:1450979-69-7
Molecular Formula:C₂₃H₁₉Cl₂F₃N₆O₂S
Molecular Weight:571.41
Hs Code.:

Synonyms:N-{1-[8-(2-chlorophenyl)-9-(4-chlorophenyl)-9H-purin-6-yl]piperidin-4-yl}-1,1,1-trifluoromethanesulfonamide

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Chemical Property of N-{1-[8-(2-chlorophenyl)-9-(4-chlorophenyl)-9H-purin-6-yl]piperidin-4-yl}-1,1,1-trifluoromethanesulfonamide

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Technology Process of N-{1-[8-(2-chlorophenyl)-9-(4-chlorophenyl)-9H-purin-6-yl]piperidin-4-yl}-1,1,1-trifluoromethanesulfonamide

There total 4 articles about N-{1-[8-(2-chlorophenyl)-9-(4-chlorophenyl)-9H-purin-6-yl]piperidin-4-yl}-1,1,1-trifluoromethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1408075-34-2
1-[8-(2-chlorophenyl)-9-(4-chlorophenyl)-9H-purin-6-yl]-piperidin-4-amine

: 1450979-69-7
N-{1-[8-(2-chlorophenyl)-9-(4-chlorophenyl)-9H-purin-6-yl]piperidin-4-yl}-1,1,1-trifluoromethanesulfonamide

Guidance literature:: With triethylamine; In dichloromethane; for 16h;

Reference yield:

: 1408075-33-1
tert-butyl N-{1-[8-(2-chlorophenyl)-9-(4-chlorophenyl)-9H-purin-6-yl]piperidin-4-yl}carbamate

: 1450979-69-7
N-{1-[8-(2-chlorophenyl)-9-(4-chlorophenyl)-9H-purin-6-yl]piperidin-4-yl}-1,1,1-trifluoromethanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 16 h

2: triethylamine / dichloromethane / 16 h

With triethylamine; trifluoroacetic acid; In dichloromethane;

Reference yield:

: 686344-50-3
6-chloro-9-(4-chlorophenyl)-8-(2-chlorophenyl)-9H-purine

: 1450979-69-7
N-{1-[8-(2-chlorophenyl)-9-(4-chlorophenyl)-9H-purin-6-yl]piperidin-4-yl}-1,1,1-trifluoromethanesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 16 h / 80 °C

2: trifluoroacetic acid / dichloromethane / 16 h

3: triethylamine / dichloromethane / 16 h

With triethylamine; trifluoroacetic acid; In ethanol; dichloromethane;