C₄₅H₄₂ClN₄O₁₃P

Base Information

• Chemical Name: C₄₅H₄₂ClN₄O₁₃P
• CAS No.: 80668-00-4
• Molecular Formula: C₄₅H₄₂ClN₄O₁₃P
• Molecular Weight: 913.274
• Mol file: 80668-00-4.mol

Synonyms:C₄₅H₄₂ClN₄O₁₃P

Chemical Property of C₄₅H₄₂ClN₄O₁₃P

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₅H₄₂ClN₄O₁₃P

There total 12 articles about C₄₅H₄₂ClN₄O₁₃P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C59H52ClN4O13P → C45H42ClN4O13P (80668-00-4)

Guidance literature:

With triethylamine; In pyridine; at 20 ℃; for 1.5h;

DOI:10.1039/c39820000672

Reference yield: 94.0%

C54H50ClN4O17PS (80667-99-8) → C45H42ClN4O13P (80668-00-4)

Guidance literature:

With triethylamine; In pyridine; at 20 ℃; for 20h; 0.04M aq. K₂CO₃, dioxane, 20 deg C, 6 min.;

DOI:10.1016/S0040-4039(01)81988-2

Reference yield:

pixyl chloride (42506-03-6) → C45H42ClN4O13P (80668-00-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent

2: 94 percent / Triethylamine / pyridine / 20 h / 20 °C / 0.04M aq. K₂CO₃, dioxane, 20 deg C, 6 min.

With triethylamine; In pyridine;

DOI:10.1016/S0040-4039(01)81988-2

upstream raw materials:

C₅₄H₅₀ClN₄O₁₇PS

pixyl chloride

3'-O-levulinoylthymidine

Carbonic acid (2R,3S,5R)-2-hydroxymethyl-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 2-trimethylsilanyl-ethyl ester