(3-(4-methoxybenzyl)-5-deuteropent-4-ynyloxy)(tert-butyl)diphenylsilane

Base Information

Chemical Name:(3-(4-methoxybenzyl)-5-deuteropent-4-ynyloxy)(tert-butyl)diphenylsilane
CAS No.:1384881-86-0
Molecular Formula:C₂₉H₃₄O₂Si
Molecular Weight:443.665
Hs Code.:

Synonyms:(3-(4-methoxybenzyl)-5-deuteropent-4-ynyloxy)(tert-butyl)diphenylsilane

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Chemical Property of (3-(4-methoxybenzyl)-5-deuteropent-4-ynyloxy)(tert-butyl)diphenylsilane

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Technology Process of (3-(4-methoxybenzyl)-5-deuteropent-4-ynyloxy)(tert-butyl)diphenylsilane

There total 5 articles about (3-(4-methoxybenzyl)-5-deuteropent-4-ynyloxy)(tert-butyl)diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1384881-85-9
(3-(4-methoxybenzyl)pent-4-ynyloxy)(tert-butyl)diphenylsilane

: 1384881-86-0
(3-(4-methoxybenzyl)-5-deuteropent-4-ynyloxy)(tert-butyl)diphenylsilane

Guidance literature:: (3-(4-methoxybenzyl)pent-4-ynyloxy)(tert-butyl)diphenylsilane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h; Inert atmosphere;

With water-d2; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ja3034075

Reference yield:

: C₁₂H₁₆O₃

: 1384881-86-0
(3-(4-methoxybenzyl)-5-deuteropent-4-ynyloxy)(tert-butyl)diphenylsilane

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / tetrahydrofuran; methanol / 16 h / 20 °C / Inert atmosphere

2.1: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 0 - 20 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere

3.2: 16 h / -78 - 20 °C / Inert atmosphere

With 1H-imidazole; n-butyllithium; potassium carbonate; In tetrahydrofuran; methanol; hexane; N,N-dimethyl-formamide;
DOI:10.1021/ja3034075

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1384881-86-0
(3-(4-methoxybenzyl)-5-deuteropent-4-ynyloxy)(tert-butyl)diphenylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere

2.2: 16 h / -78 - 20 °C / Inert atmosphere

With 1H-imidazole; n-butyllithium; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1021/ja3034075