6-Benzyloxy-3-[4-(hydroxymethyl)-3-(methyl)benzyl]-2-[4-[2-(1-pyrrolidinyl)ethoxy]phenyl]benzo[b]thiophene

Base Information

Chemical Name:6-Benzyloxy-3-[4-(hydroxymethyl)-3-(methyl)benzyl]-2-[4-[2-(1-pyrrolidinyl)ethoxy]phenyl]benzo[b]thiophene
CAS No.:215587-31-8
Molecular Formula:C₃₆H₃₇NO₃S
Molecular Weight:563.761
Hs Code.:

Synonyms:6-Benzyloxy-3-[4-(hydroxymethyl)-3-(methyl)benzyl]-2-[4-[2-(1-pyrrolidinyl)ethoxy]phenyl]benzo[b]thiophene

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Chemical Property of 6-Benzyloxy-3-[4-(hydroxymethyl)-3-(methyl)benzyl]-2-[4-[2-(1-pyrrolidinyl)ethoxy]phenyl]benzo[b]thiophene

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Technology Process of 6-Benzyloxy-3-[4-(hydroxymethyl)-3-(methyl)benzyl]-2-[4-[2-(1-pyrrolidinyl)ethoxy]phenyl]benzo[b]thiophene

There total 1 articles about 6-Benzyloxy-3-[4-(hydroxymethyl)-3-(methyl)benzyl]-2-[4-[2-(1-pyrrolidinyl)ethoxy]phenyl]benzo[b]thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 215587-31-8
6-Benzyloxy-3-[4-(hydroxymethyl)-3-(methyl)benzyl]-2-[4-[2-(1-pyrrolidinyl)ethoxy]phenyl]benzo[b]thiophene

Guidance literature:

Reference yield: 62.0%

: 215587-31-8
6-Benzyloxy-3-[4-(hydroxymethyl)-3-(methyl)benzyl]-2-[4-[2-(1-pyrrolidinyl)ethoxy]phenyl]benzo[b]thiophene

: 3195-95-7
sodium salt of 2-pyrrolidinone

: 215605-52-0
6-benzyloxy-3-[3-methyl-4-[(2-oxopyrrolidin-1-yl)methyl]benzyl]-2-[4-[2-(1-pyrrolidinyl)ethoxy]phenyl]benzo[b] thiophene

Guidance literature:: 6-Benzyloxy-3-[4-(hydroxymethyl)-3-(methyl)benzyl]-2-[4-[2-(1-pyrrolidinyl)ethoxy]phenyl]benzo[b]thiophene; With n-butyllithium; In tetrahydrofuran; hexanes; at 0 ℃; for 0.25h;

With methanesulfonyl chloride; In tetrahydrofuran; at 0 ℃; for 1.5h;

sodium salt of 2-pyrrolidinone; In tetrahydrofuran; at 0 - 20 ℃; for 17.75h;

Reference yield: 26.0%

: 215587-31-8
6-Benzyloxy-3-[4-(hydroxymethyl)-3-(methyl)benzyl]-2-[4-[2-(1-pyrrolidinyl)ethoxy]phenyl]benzo[b]thiophene

: 33081-78-6
sodium phthalimide

: 6-benzyloxy-3-[3-methyl-4-[(1-phthalimidyl)methyl]benzyl]-2-[4-[2-(1-pyrrolidinyl)ethoxy]phenyl]benzo[b]thiophene

Guidance literature:: 6-Benzyloxy-3-[4-(hydroxymethyl)-3-(methyl)benzyl]-2-[4-[2-(1-pyrrolidinyl)ethoxy]phenyl]benzo[b]thiophene; With methanesulfonyl chloride; triethylamine; In dichloromethane; at 0 ℃; for 1h;

sodium phthalimide; With lithium iodide; at 0 - 20 ℃; for 4h;