(-)- acetate d'isopropenyl-3 heptene-6 yle (3R)

Base Information

Chemical Name:(-)- acetate d'isopropenyl-3 heptene-6 yle (3R)
CAS No.:125318-15-2
Molecular Formula:C₂₀H₂₅F₃O₃
Molecular Weight:370.412
Hs Code.:

(-)-<methoxy-2 phenyl-2 trifluoromethyl-2S> acetate d'isopropenyl-3 heptene-6 yle (3R)

Synonyms:(-)- acetate d'isopropenyl-3 heptene-6 yle (3R)

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Chemical Property of (-)- acetate d'isopropenyl-3 heptene-6 yle (3R)

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Technology Process of (-)- acetate d'isopropenyl-3 heptene-6 yle (3R)

There total 6 articles about (-)- acetate d'isopropenyl-3 heptene-6 yle (3R) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 20445-33-4,39637-99-5
(R)-methoxytrifluoromethylphenylacetyl chloride

: 99277-16-4
(R)-3-(1-methylethenyl)-6-hepten-1-ol

: 125318-15-2
(-)- acetate d'isopropenyl-3 heptene-6 yle (3R)

Guidance literature:: With pyridine; In tetrachloromethane; at 25 ℃; for 5h;
DOI:10.1016/S0040-4020(01)80068-5

Reference yield:

: 67169-07-7
(R)-3-(1-methylethenyl)-6-heptenal

: 125318-15-2
(-)- acetate d'isopropenyl-3 heptene-6 yle (3R)

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether / 0.5 h / 0 °C

2: 86 percent / pyridine / CCl₄ / 5 h / 25 °C

With pyridine; lithium aluminium tetrahydride; In tetrachloromethane; diethyl ether;
DOI:10.1016/S0040-4020(01)80068-5

Reference yield:

: 5989-27-5,555-08-8,8022-90-0,9003-73-0,95327-98-3
D-limonene

: 125318-15-2
(-)- acetate d'isopropenyl-3 heptene-6 yle (3R)

Guidance literature:: Multi-step reaction with 6 steps

2: iPr₂NLi / tetrahydrofuran

3: 72 percent / Li / liquid ammonia; tetrahydrofuran / 0.17 h / -78 °C

4: 35percent HClO₄ / tetrahydrofuran; H₂O / 4 h / Ambient temperature

5: LiAlH₄ / diethyl ether / 0.5 h / 0 °C

6: 86 percent / pyridine / CCl₄ / 5 h / 25 °C

With pyridine; lithium aluminium tetrahydride; perchloric acid; lithium; lithium diisopropyl amide; In tetrahydrofuran; tetrachloromethane; diethyl ether; ammonia; water;
DOI:10.1016/S0040-4020(01)80068-5