N-((7,7-dimethylcyclohept-1-enyl)methyl)-3-fluoroaniline hydrochloride

Base Information

Chemical Name:N-((7,7-dimethylcyclohept-1-enyl)methyl)-3-fluoroaniline hydrochloride
CAS No.:1441168-46-2
Molecular Formula:C₁₆H₂₂FN*ClH
Molecular Weight:283.817
Hs Code.:

Synonyms:N-((7,7-dimethylcyclohept-1-enyl)methyl)-3-fluoroaniline hydrochloride

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Chemical Property of N-((7,7-dimethylcyclohept-1-enyl)methyl)-3-fluoroaniline hydrochloride

Chemical Property:

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Technology Process of N-((7,7-dimethylcyclohept-1-enyl)methyl)-3-fluoroaniline hydrochloride

There total 7 articles about N-((7,7-dimethylcyclohept-1-enyl)methyl)-3-fluoroaniline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1441169-61-4
N-((7,7-dimethylcyclohept-1-enyl)methyl)-3-fluoroaniline

: 1441168-46-2
N-((7,7-dimethylcyclohept-1-enyl)methyl)-3-fluoroaniline hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether; at 20 ℃; for 2h;

Reference yield:

: 1439355-94-8
(E)-7-(isopropoxymethylene)-2,2-dimethylcycloheptanone

: 1441168-46-2
N-((7,7-dimethylcyclohept-1-enyl)methyl)-3-fluoroaniline hydrochloride

Guidance literature:: Multi-step reaction with 7 steps

1: sodium hydroxide / water; ethanol / 9 h / Reflux

2: zinc(II) iodide / dichloromethane / 2 h / 20 °C

3: hydrogenchloride / tetrahydrofuran; water / 20 °C

4: thionyl chloride; pyridine / 2 h / 20 °C

5: diisobutylaluminium hydride / dichloromethane; hexane / 2 h / -78 °C / Inert atmosphere

6: acetic acid; sodium cyanoborohydride / methanol / 2 h / 20 °C

7: hydrogenchloride / diethyl ether / 2 h / 20 °C

With pyridine; hydrogenchloride; thionyl chloride; diisobutylaluminium hydride; sodium cyanoborohydride; acetic acid; sodium hydroxide; zinc(II) iodide; In tetrahydrofuran; methanol; diethyl ether; ethanol; hexane; dichloromethane; water;

Reference yield:

: 1439355-96-0
2,2-dimethyl-1-(trimethylsilyloxy)cycloheptanecarbonitrile

: 1441168-46-2
N-((7,7-dimethylcyclohept-1-enyl)methyl)-3-fluoroaniline hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride / tetrahydrofuran; water / 20 °C

2: thionyl chloride; pyridine / 2 h / 20 °C

3: diisobutylaluminium hydride / dichloromethane; hexane / 2 h / -78 °C / Inert atmosphere

4: acetic acid; sodium cyanoborohydride / methanol / 2 h / 20 °C

5: hydrogenchloride / diethyl ether / 2 h / 20 °C

With pyridine; hydrogenchloride; thionyl chloride; diisobutylaluminium hydride; sodium cyanoborohydride; acetic acid; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water;