3-(1',3'-dihydroxy-3',7'-dimethyl-oct-6'-en-1'-yl)-4-hydroxybenzoic acid

Base Information

Chemical Name:3-(1',3'-dihydroxy-3',7'-dimethyl-oct-6'-en-1'-yl)-4-hydroxybenzoic acid
CAS No.:1326774-92-8
Molecular Formula:C₁₇H₂₄O₅
Molecular Weight:308.375
Hs Code.:

Synonyms:3-(1',3'-dihydroxy-3',7'-dimethyl-oct-6'-en-1'-yl)-4-hydroxybenzoic acid

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Chemical Property of 3-(1',3'-dihydroxy-3',7'-dimethyl-oct-6'-en-1'-yl)-4-hydroxybenzoic acid

Chemical Property:

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Technology Process of 3-(1',3'-dihydroxy-3',7'-dimethyl-oct-6'-en-1'-yl)-4-hydroxybenzoic acid

There total 5 articles about 3-(1',3'-dihydroxy-3',7'-dimethyl-oct-6'-en-1'-yl)-4-hydroxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1326774-91-7
3-(1',3'-dihydroxy-3',7'-dimethyl-oct-6'-en-1'-yl)-4-hydroxybenzoic acid methyl ester

: 1326774-92-8
3-(1',3'-dihydroxy-3',7'-dimethyl-oct-6'-en-1'-yl)-4-hydroxybenzoic acid

Guidance literature:: With lithium hydroxide monohydrate; In tetrahydrofuran; water; for 9h; Reflux; Inert atmosphere;
DOI:10.1002/cbdv.201100288

Reference yield:

: 1326774-90-6
4-hydroxy-3-(3'-hydroxy-3',7'-dimethyl-oct-6'-enoyl)benzoic acid methyl ester

: 1326774-92-8
3-(1',3'-dihydroxy-3',7'-dimethyl-oct-6'-en-1'-yl)-4-hydroxybenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate / methanol / 2 h / 0 - 20 °C

2.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 9 h / Reflux

2.2: 0 °C / pH 3

With sodium tetrahydroborate; lithium hydroxide monohydrate; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.tet.2011.06.015

Reference yield:

: 57009-12-8
methyl 3-acetyl-4-hydroxybenzoate

: 1326774-92-8
3-(1',3'-dihydroxy-3',7'-dimethyl-oct-6'-en-1'-yl)-4-hydroxybenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; n-heptane / 1.17 h / -78 °C / Inert atmosphere

1.2: 3 h / -78 °C / Inert atmosphere

1.3: -78 °C

2.1: sodium tetrahydroborate / methanol / 2 h / 0 - 20 °C

3.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 9 h / Reflux

3.2: 0 °C / pH 3

With sodium tetrahydroborate; lithium hydroxide monohydrate; lithium diisopropyl amide; In tetrahydrofuran; methanol; n-heptane; water; 1.1: Aldol reaction / 1.2: Aldol reaction;
DOI:10.1016/j.tet.2011.06.015