N-phenethyl-2,2,2-trifluoroethanimidic acid 1-methylethylidene hydrazide

Base Information

• Chemical Name: N-phenethyl-2,2,2-trifluoroethanimidic acid 1-methylethylidene hydrazide
• CAS No.: 143681-50-9
• Molecular Formula: C₁₃H₁₆F₃N₃
• Molecular Weight: 271.285

Synonyms:N-phenethyl-2,2,2-trifluoroethanimidic acid 1-methylethylidene hydrazide

Chemical Property of N-phenethyl-2,2,2-trifluoroethanimidic acid 1-methylethylidene hydrazide

Chemical Property:

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Technology Process of N-phenethyl-2,2,2-trifluoroethanimidic acid 1-methylethylidene hydrazide

There total 1 articles about N-phenethyl-2,2,2-trifluoroethanimidic acid 1-methylethylidene hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

N-Phenethyl-2,2,2-trifluoroacetimidoyl chloride (143681-39-4) + propan-2-one azine (627-70-3) → N-phenethyl-2,2,2-trifluoroethanimidic acid 1-methylethylidene hydrazide (143681-50-9)

Guidance literature:

With hydrazine hydrate; In water; N,N-dimethyl-formamide; for 5h; Ambient temperature;

DOI:10.1021/jo00048a042

Reference yield: 78.0%

N-phenethyl-2,2,2-trifluoroethanimidic acid 1-methylethylidene hydrazide (143681-50-9) → 1-(1-chloro-1-methylethyl)-3-(trifluoromethyl)-5-benzyl-1,2,4-triazole (143681-64-5)

Guidance literature:

With tert-butylhypochlorite; In dichloromethane; for 7h; Ambient temperature;

DOI:10.1021/jo00048a042

Reference yield: 44.0%

N-phenethyl-2,2,2-trifluoroethanimidic acid 1-methylethylidene hydrazide (143681-50-9) → 3-(trifluoromethyl)-5-benzyl-1,2,4-triazole (143681-62-3)

Guidance literature:

With tert-butylhypochlorite; In dichloromethane; for 7h; Ambient temperature;

DOI:10.1021/jo00048a042

upstream raw materials:

N-Phenethyl-2,2,2-trifluoroacetimidoyl chloride

propan-2-one azine

Downstream raw materials:

3-(trifluoromethyl)-5-benzyl-1,2,4-triazole

1-(1-chloro-1-methylethyl)-3-(trifluoromethyl)-5-benzyl-1,2,4-triazole

1-(1-methylethenyl)-3-(trifluoromethyl)-5-benzyl-1,2,4-triazole

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