benzyl 2-benzyl-6-ethyl-4-oxopiperidine-1-carboxylate

Base Information

Chemical Name:benzyl 2-benzyl-6-ethyl-4-oxopiperidine-1-carboxylate
CAS No.:1003843-26-2
Molecular Formula:C₂₂H₂₅NO₃
Molecular Weight:351.445
Hs Code.:

Synonyms:benzyl 2-benzyl-6-ethyl-4-oxopiperidine-1-carboxylate

Suppliers and Price of benzyl 2-benzyl-6-ethyl-4-oxopiperidine-1-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 2-benzyl-6-ethyl-4-oxopiperidine-1-carboxylate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of benzyl 2-benzyl-6-ethyl-4-oxopiperidine-1-carboxylate

There total 1 articles about benzyl 2-benzyl-6-ethyl-4-oxopiperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 150708-76-2
2-benzyl-4-oxo-3,4-dihydro-2H-pyridine-1-carboxylic acid benzyl ester

: 1003843-26-2
benzyl 2-benzyl-6-ethyl-4-oxopiperidine-1-carboxylate

Guidance literature:: ethylmagnesium bromide; With copper(l) iodide; In tetrahydrofuran; at -78 ℃; for 0.166667h;

With boron trifluoride diethyl etherate; In tetrahydrofuran; at -78 ℃; for 0.166667h;

2-benzyl-4-oxo-3,4-dihydro-2H-pyridine-1-carboxylic acid benzyl ester; With water; ammonium chloride; more than 3 stages;

Reference yield: 74.0%

: 1003843-26-2
benzyl 2-benzyl-6-ethyl-4-oxopiperidine-1-carboxylate

: rac-(2S,6R)-2-benzyl-6-ethylpiperidin-4-one

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃;
DOI:10.1021/acs.jmedchem.7b00900

Reference yield: 51.0%

: 1003843-26-2
benzyl 2-benzyl-6-ethyl-4-oxopiperidine-1-carboxylate

: 85068-29-7
3,5-bis-trifluoromethylbenzylamine

: 2-benzyl-4-(3,5-bis-trifluoromethyl-benzylamino)-6-ethyl-piperidine-1-carboxylic acid benzyl ester

Guidance literature:: benzyl 2-benzyl-6-ethyl-4-oxopiperidine-1-carboxylate; 3,5-bis-trifluoromethylbenzylamine; With sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane; at 20 ℃; for 15h;

With sodium hydroxide; water; In 1,2-dichloro-ethane; pH=~ 10;