C₂₇H₄₃ClN₄O₄

Base Information

Chemical Name:C₂₇H₄₃ClN₄O₄
CAS No.:1436429-24-1
Molecular Formula:C₂₇H₄₃ClN₄O₄
Molecular Weight:523.116
Hs Code.:

C<sub>27</sub>H<sub>43</sub>ClN<sub>4</sub>O<sub>4</sub>

Synonyms:C₂₇H₄₃ClN₄O₄

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Chemical Property of C₂₇H₄₃ClN₄O₄

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Technology Process of C₂₇H₄₃ClN₄O₄

There total 13 articles about C₂₇H₄₃ClN₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₂H₅₁ClN₄O₆

: 110-17-8,26099-09-2
(2E)-but-2-enedioic acid

: 1436429-24-1
C₂₇H₄₃ClN₄O₄

Guidance literature:: C₃₂H₅₁ClN₄O₆; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.833333h;

(2E)-but-2-enedioic acid; In methanol; at 20 ℃; for 0.0833333h;
DOI:10.1016/j.bmc.2013.03.022

Reference yield:

: 1000052-56-1
(2R,4E)-6-(benzyloxy)-2-ethylhex-4-enoic acid

: 1436429-24-1
C₂₇H₄₃ClN₄O₄

Guidance literature:: Multi-step reaction with 11 steps

1.1: tetra(n-butyl)ammonium hydrogensulfate; Shi's ketone; Oxone; potassium carbonate; edetate disodium / acetonitrile / 9 h / 0 °C

2.1: triethylamine / dichloromethane / 3 h / 0 °C

3.1: sodium azide; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone / 72 h / 60 °C

4.1: hydrogenchloride; palladium 10% on activated carbon; hydrogen / ethanol; 1,4-dioxane / 6 h / 20 °C

5.1: triethylamine / tetrahydrofuran; water / 2 h / 0 °C

6.1: diethylazodicarboxylate; triphenylphosphine / tetrahydrofuran; toluene / 0.17 h / 0 °C

7.1: toluene / 1.5 h / 110 °C

8.1: caesium carbonate; thiophenol / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

9.1: triethylamine / dichloromethane / 15 h / 20 °C

10.1: triethylamine; 2-hydroxypyridin / 18 h / 80 °C

11.1: trifluoroacetic acid / dichloromethane / 0.83 h / 20 °C

11.2: 0.08 h / 20 °C

With 2-hydroxypyridin; hydrogenchloride; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; Oxone; sodium azide; Shi's ketone; palladium 10% on activated carbon; hydrogen; tetra(n-butyl)ammonium hydrogensulfate; edetate disodium; potassium carbonate; caesium carbonate; thiophenol; triethylamine; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 1.1: |Shi Asymmetric Epoxidation / 6.1: |Mitsunobu Displacement;
DOI:10.1016/j.bmc.2013.03.022

Reference yield:

: 1000052-53-8
(4S)-4-benzyl-3-[(2R,4E)-6-(benzyloxy)-2-ethylhex-4-enoyl]-1,3-oxazolidin-2-one

: 1436429-24-1
C₂₇H₄₃ClN₄O₄

Guidance literature:: Multi-step reaction with 12 steps

1.1: dihydrogen peroxide; lithium hydroxide monohydrate / tetrahydrofuran; water / 16.5 h / 0 - 20 °C

2.1: tetra(n-butyl)ammonium hydrogensulfate; Shi's ketone; Oxone; potassium carbonate; edetate disodium / acetonitrile / 9 h / 0 °C

3.1: triethylamine / dichloromethane / 3 h / 0 °C

4.1: sodium azide; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone / 72 h / 60 °C

5.1: hydrogenchloride; palladium 10% on activated carbon; hydrogen / ethanol; 1,4-dioxane / 6 h / 20 °C

6.1: triethylamine / tetrahydrofuran; water / 2 h / 0 °C

7.1: diethylazodicarboxylate; triphenylphosphine / tetrahydrofuran; toluene / 0.17 h / 0 °C

8.1: toluene / 1.5 h / 110 °C

9.1: caesium carbonate; thiophenol / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

10.1: triethylamine / dichloromethane / 15 h / 20 °C

11.1: triethylamine; 2-hydroxypyridin / 18 h / 80 °C

12.1: trifluoroacetic acid / dichloromethane / 0.83 h / 20 °C

12.2: 0.08 h / 20 °C

With 2-hydroxypyridin; hydrogenchloride; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; Oxone; sodium azide; Shi's ketone; lithium hydroxide monohydrate; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; tetra(n-butyl)ammonium hydrogensulfate; edetate disodium; potassium carbonate; caesium carbonate; thiophenol; triethylamine; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 2.1: |Shi Asymmetric Epoxidation / 7.1: |Mitsunobu Displacement;
DOI:10.1016/j.bmc.2013.03.022