C₃₃H₃₄F₇NOSSeSi

Base Information

Chemical Name:C₃₃H₃₄F₇NOSSeSi
CAS No.:1332495-16-5
Molecular Formula:C₃₃H₃₄F₇NOSSeSi
Molecular Weight:732.739
Hs Code.:

C<sub>33</sub>H<sub>34</sub>F<sub>7</sub>NOSSeSi

Synonyms:C₃₃H₃₄F₇NOSSeSi

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Chemical Property of C₃₃H₃₄F₇NOSSeSi

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Technology Process of C₃₃H₃₄F₇NOSSeSi

There total 7 articles about C₃₃H₃₄F₇NOSSeSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1332494-96-8
C₂₅H₃₀F₃NOSSeSi

: 239087-08-2
2-(bromomethyl)-1-fluoro-3-(trifluoromethyl)benzene

: 1332495-16-5
C₃₃H₃₄F₇NOSSeSi

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -78 - 20 ℃; for 0.5h;

Reference yield:

: 455-18-5
4-CF₃C₆H₄CN

: 1332495-16-5
C₃₃H₃₄F₇NOSSeSi

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogenchloride; selenium; pyridine; sodium tetrahydroborate / ethanol; water / 1.5 h / 80 °C / Inert atmosphere

2.1: tetrahydrofuran / 12.83 h / 20 - 80 °C

3.1: diisobutylaluminium hydride / dichloromethane; hexane / 1.5 h / -78 - -10 °C / Inert atmosphere

4.1: N-chloro-succinimide; triphenylphosphine / dichloromethane / 1 h / 20 °C

5.1: isopropylmagnesium chloride / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

5.2: 0.17 h / -78 °C

6.1: 1H-imidazole / N,N-dimethyl-formamide / 4 h / 20 °C

7.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 - 20 °C

With pyridine; 1H-imidazole; hydrogenchloride; selenium; sodium tetrahydroborate; N-chloro-succinimide; isopropylmagnesium chloride; diisobutylaluminium hydride; triphenylphosphine; lithium diisopropyl amide; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1332498-00-6
C₁₂H₁₀F₃NOSe

: 1332495-16-5
C₃₃H₃₄F₇NOSSeSi

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-chloro-succinimide; triphenylphosphine / dichloromethane / 1 h / 20 °C

2.1: isopropylmagnesium chloride / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

2.2: 0.17 h / -78 °C

3.1: 1H-imidazole / N,N-dimethyl-formamide / 4 h / 20 °C

4.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 - 20 °C

With 1H-imidazole; N-chloro-succinimide; isopropylmagnesium chloride; triphenylphosphine; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;