[1-(Hydroxy-methoxy-phosphoryl)-2,3-diphenyl-cycloprop-2-enyl]-phosphonic acid monomethyl ester

Base Information

Chemical Name:[1-(Hydroxy-methoxy-phosphoryl)-2,3-diphenyl-cycloprop-2-enyl]-phosphonic acid monomethyl ester
CAS No.:138849-73-7
Molecular Formula:C₁₇H₁₈O₆P₂
Molecular Weight:380.274
Hs Code.:

Synonyms:[1-(Hydroxy-methoxy-phosphoryl)-2,3-diphenyl-cycloprop-2-enyl]-phosphonic acid monomethyl ester

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Chemical Property of [1-(Hydroxy-methoxy-phosphoryl)-2,3-diphenyl-cycloprop-2-enyl]-phosphonic acid monomethyl ester

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Technology Process of [1-(Hydroxy-methoxy-phosphoryl)-2,3-diphenyl-cycloprop-2-enyl]-phosphonic acid monomethyl ester

There total 3 articles about [1-(Hydroxy-methoxy-phosphoryl)-2,3-diphenyl-cycloprop-2-enyl]-phosphonic acid monomethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 138849-66-8
3,3-Bis(dimethoxyphosphinyl)-1,2-diphenylcyclopropene

: 138849-73-7
[1-(Hydroxy-methoxy-phosphoryl)-2,3-diphenyl-cycloprop-2-enyl]-phosphonic acid monomethyl ester

Guidance literature:: With sodium hydroxide; In ethanol; at 50 ℃; for 5h;
DOI:10.1246/bcsj.64.3476

Reference yield:

: 138849-74-8
1,2-Diphenyl-3,3-dibromocyclopropene

: 138849-73-7
[1-(Hydroxy-methoxy-phosphoryl)-2,3-diphenyl-cycloprop-2-enyl]-phosphonic acid monomethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 17 percent / CH₂Cl₂ / 24 h / 40 °C

2: 88 percent / NaOH / ethanol / 5 h / 50 °C

With sodium hydroxide; In ethanol; dichloromethane;
DOI:10.1246/bcsj.64.3476

Reference yield:

: 886-38-4
diphenylcyclopropenone

: 138849-73-7
[1-(Hydroxy-methoxy-phosphoryl)-2,3-diphenyl-cycloprop-2-enyl]-phosphonic acid monomethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: SOBr₂ / CH₂Cl₂ / 0.17 h / Ambient temperature

2: 17 percent / CH₂Cl₂ / 24 h / 40 °C

3: 88 percent / NaOH / ethanol / 5 h / 50 °C

With sodium hydroxide; sulfurous dibromide; In ethanol; dichloromethane;
DOI:10.1246/bcsj.64.3476