1-cyclohexylmethyl-3-(2,6-diisopropylphenyl)-4,5-dihydro-1H-imidazol-3-ium chloride

Base Information

• Chemical Name: 1-cyclohexylmethyl-3-(2,6-diisopropylphenyl)-4,5-dihydro-1H-imidazol-3-ium chloride
• CAS No.: 1299294-15-7
• Molecular Formula: C₂₂H₃₅N₂*Cl
• Molecular Weight: 362.986
• Mol file: 1299294-15-7.mol

Synonyms:1-cyclohexylmethyl-3-(2,6-diisopropylphenyl)-4,5-dihydro-1H-imidazol-3-ium chloride

Chemical Property of 1-cyclohexylmethyl-3-(2,6-diisopropylphenyl)-4,5-dihydro-1H-imidazol-3-ium chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-cyclohexylmethyl-3-(2,6-diisopropylphenyl)-4,5-dihydro-1H-imidazol-3-ium chloride

There total 4 articles about 1-cyclohexylmethyl-3-(2,6-diisopropylphenyl)-4,5-dihydro-1H-imidazol-3-ium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

N1-cyclohexylmethyl-N2-(2,6-diisopropylphenyl)ethane-1,2-diamine (1299294-14-6) + orthoformic acid triethyl ester (122-51-0) → 1-cyclohexylmethyl-3-(2,6-diisopropylphenyl)-4,5-dihydro-1H-imidazol-3-ium chloride (1299294-15-7)

Guidance literature:

With ammonium chloride; Reflux;

Reference yield:

N1-(2,6-diisopropylphenyl)ethane-1,2-diamine (888705-44-0) → 1-cyclohexylmethyl-3-(2,6-diisopropylphenyl)-4,5-dihydro-1H-imidazol-3-ium chloride (1299294-15-7)

Guidance literature:

Multi-step reaction with 3 steps

1: benzene / 1.5 h / Reflux

2: sodium tetrahydroborate / tetrahydrofuran / 0.5 h / Reflux

3: ammonium chloride / Reflux

With sodium tetrahydroborate; ammonium chloride; In tetrahydrofuran; benzene;

Reference yield:

N1-cyclohexylmethylene-N2-(2,6-diisopropylphenyl)ethane-1,2-diamine (1299294-13-5) → 1-cyclohexylmethyl-3-(2,6-diisopropylphenyl)-4,5-dihydro-1H-imidazol-3-ium chloride (1299294-15-7)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium tetrahydroborate / tetrahydrofuran / 0.5 h / Reflux

2: ammonium chloride / Reflux

With sodium tetrahydroborate; ammonium chloride; In tetrahydrofuran;

upstream raw materials:

2,6-diisopropylbenzenamine

N₁-cyclohexylmethyl-N₂-(2,6-diisopropylphenyl)ethane-1,2-diamine

orthoformic acid triethyl ester

N¹-(2,6-diisopropylphenyl)ethane-1,2-diamine