Technology Process of C11H12N4O
There total 3 articles about C11H12N4O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trimethylsilylazide; copper diacetate; sodium acetate;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 24h;
Reagent/catalyst;
Time;
Inert atmosphere;
DOI:10.1021/ol403687k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Jones reagent / diethyl ether / 0 - 20 °C / Inert atmosphere
2: hydroxylamine hydrochloride; sodium acetate / water; ethanol / 20 °C / Inert atmosphere
3: trimethylsilylazide; copper diacetate; sodium acetate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere
With
Jones reagent; trimethylsilylazide; hydroxylamine hydrochloride; copper diacetate; sodium acetate;
In
diethyl ether; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ol403687k
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydroxylamine hydrochloride; sodium acetate / water; ethanol / 20 °C / Inert atmosphere
2: trimethylsilylazide; copper diacetate; sodium acetate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere
With
trimethylsilylazide; hydroxylamine hydrochloride; copper diacetate; sodium acetate;
In
ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ol403687k