2-(allylsulfanyl)-5-methoxy-1-(4-methoxyphenyl)-1H-3-pyrrolcarbaldehyde

Base Information

Chemical Name:2-(allylsulfanyl)-5-methoxy-1-(4-methoxyphenyl)-1H-3-pyrrolcarbaldehyde
CAS No.:280576-55-8
Molecular Formula:C₁₆H₁₇NO₃S
Molecular Weight:303.382
Hs Code.:

Synonyms:2-(allylsulfanyl)-5-methoxy-1-(4-methoxyphenyl)-1H-3-pyrrolcarbaldehyde

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Chemical Property of 2-(allylsulfanyl)-5-methoxy-1-(4-methoxyphenyl)-1H-3-pyrrolcarbaldehyde

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Technology Process of 2-(allylsulfanyl)-5-methoxy-1-(4-methoxyphenyl)-1H-3-pyrrolcarbaldehyde

There total 2 articles about 2-(allylsulfanyl)-5-methoxy-1-(4-methoxyphenyl)-1H-3-pyrrolcarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (4-methoxy-phenyl)-(1-methoxy-vinyl)-amine

: 280576-55-8
2-(allylsulfanyl)-5-methoxy-1-(4-methoxyphenyl)-1H-3-pyrrolcarbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: 82 percent / Et₃N / diethyl ether / 2 h / 0 °C

2.1: 69 percent / POCl₃

3.1: ethanol / 1 h / Heating

3.2: NaOH / ethanol / 1 h / Heating

3.3: 74 percent / NaOH / ethanol / 0.5 h

With triethylamine; trichlorophosphate; In diethyl ether; ethanol; 1.1: Cyclization / 2.1: chloroformylation / 3.1: Alkylation / 3.2: Hydrolysis / 3.3: Condensation;
DOI:10.1016/S0040-4020(00)00056-9

Reference yield:

: 280576-46-7
5-methoxy-1-(4-methoxyphenyl)-2,3-dihydro-1H-2-pyrrolone

: 280576-55-8
2-(allylsulfanyl)-5-methoxy-1-(4-methoxyphenyl)-1H-3-pyrrolcarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: 69 percent / POCl₃

2.1: ethanol / 1 h / Heating

2.2: NaOH / ethanol / 1 h / Heating

2.3: 74 percent / NaOH / ethanol / 0.5 h

With trichlorophosphate; In ethanol; 1.1: chloroformylation / 2.1: Alkylation / 2.2: Hydrolysis / 2.3: Condensation;
DOI:10.1016/S0040-4020(00)00056-9

Reference yield: 68.0%

: 280576-55-8
2-(allylsulfanyl)-5-methoxy-1-(4-methoxyphenyl)-1H-3-pyrrolcarbaldehyde

: 280576-60-5
2-(allylsulfanyl)-5-methoxy-1-(4-methoxyphenyl)-1H-3-pyrrolcarbaldehydeoxime

Guidance literature:: With hydroxylamine hydrochloride; sodium hydrogencarbonate; In ethanol; water; at 20 ℃;
DOI:10.1016/S0040-4020(00)00056-9