methyl 4-(3-(5-(4-(mesitylsulfonyl)piperazin-1-yl)pyridin-2-yl)-4-oxothiazolidin-2-yl)-3-methoxybenzoate

Base Information

Chemical Name:methyl 4-(3-(5-(4-(mesitylsulfonyl)piperazin-1-yl)pyridin-2-yl)-4-oxothiazolidin-2-yl)-3-methoxybenzoate
CAS No.:1615687-46-1
Molecular Formula:C₃₀H₃₄N₄O₆S₂
Molecular Weight:610.755
Hs Code.:

Synonyms:methyl 4-(3-(5-(4-(mesitylsulfonyl)piperazin-1-yl)pyridin-2-yl)-4-oxothiazolidin-2-yl)-3-methoxybenzoate

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Chemical Property of methyl 4-(3-(5-(4-(mesitylsulfonyl)piperazin-1-yl)pyridin-2-yl)-4-oxothiazolidin-2-yl)-3-methoxybenzoate

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Technology Process of methyl 4-(3-(5-(4-(mesitylsulfonyl)piperazin-1-yl)pyridin-2-yl)-4-oxothiazolidin-2-yl)-3-methoxybenzoate

There total 5 articles about methyl 4-(3-(5-(4-(mesitylsulfonyl)piperazin-1-yl)pyridin-2-yl)-4-oxothiazolidin-2-yl)-3-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 773-64-8
2-mesitylenesulphonyl chloride

: 1615687-54-1
methyl 3-methoxy-4-(4-oxo-3-(5-(piperazin-1-yl)pyridin-2-yl)thiazolidin-2-yl)benzoate

: 1615687-46-1
methyl 4-(3-(5-(4-(mesitylsulfonyl)piperazin-1-yl)pyridin-2-yl)-4-oxothiazolidin-2-yl)-3-methoxybenzoate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.ejmech.2014.05.009

Reference yield:

: 571189-16-7
4-(6-nitropyridin-3-yl)-piperazine-1-carboxylic acid tert-butyl ester

: 1615687-46-1
methyl 4-(3-(5-(4-(mesitylsulfonyl)piperazin-1-yl)pyridin-2-yl)-4-oxothiazolidin-2-yl)-3-methoxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen; palladium 10% on activated carbon / ethanol / 2 h

2: 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide / ethyl acetate / 3 h / 0 - 20 °C

3: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C

4: triethylamine / dichloromethane / 0 - 20 °C

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; triethylamine; In 1,4-dioxane; ethanol; dichloromethane; ethyl acetate;
DOI:10.1016/j.ejmech.2014.05.009

Reference yield:

: 571188-59-5
tert-butyl 4-(6-aminopyridin-3-yl)piperazine-1-carboxylate

: 1615687-46-1
methyl 4-(3-(5-(4-(mesitylsulfonyl)piperazin-1-yl)pyridin-2-yl)-4-oxothiazolidin-2-yl)-3-methoxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide / ethyl acetate / 3 h / 0 - 20 °C

2: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C

3: triethylamine / dichloromethane / 0 - 20 °C

With hydrogenchloride; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; triethylamine; In 1,4-dioxane; dichloromethane; ethyl acetate;
DOI:10.1016/j.ejmech.2014.05.009