methyl 4-O-acetyl-2,3-di-O-benzyl-β-D-galactopyranosyluronate N-phenyl trifluoroacetimidate

Base Information

• Chemical Name: methyl 4-O-acetyl-2,3-di-O-benzyl-β-D-galactopyranosyluronate N-phenyl trifluoroacetimidate
• CAS No.: 1462321-84-1
• Molecular Formula: C₃₁H₃₀F₃NO₈
• Molecular Weight: 601.576
• Mol file: 1462321-84-1.mol

Synonyms:methyl 4-O-acetyl-2,3-di-O-benzyl-β-D-galactopyranosyluronate N-phenyl trifluoroacetimidate

Chemical Property of methyl 4-O-acetyl-2,3-di-O-benzyl-β-D-galactopyranosyluronate N-phenyl trifluoroacetimidate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of methyl 4-O-acetyl-2,3-di-O-benzyl-β-D-galactopyranosyluronate N-phenyl trifluoroacetimidate

There total 1 articles about methyl 4-O-acetyl-2,3-di-O-benzyl-β-D-galactopyranosyluronate N-phenyl trifluoroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2,2-trifluoro-N-phenyl-acetimidoyl chloride (61881-19-4) + methyl 4-O-acetyl-2,3-di-O-benzyl-α/β-D-galactopyranuronate → methyl 4-O-acetyl-2,3-di-O-benzyl-β-D-galactopyranosyluronate N-phenyl trifluoroacetimidate (1462321-84-1) + methyl 4-O-acetyl-2,3-di-O-benzyl-α-D-galactopyranosyluronate N-phenyl trifluoroacetimidate (1462321-83-0)

Guidance literature:

With caesium carbonate; In acetone; at 20 ℃; for 3h; Overall yield = 88 %; Overall yield = 529 mg;

DOI:10.1016/j.carres.2013.06.019

upstream raw materials:

2,2,2-trifluoro-N-phenyl-acetimidoyl chloride