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C35H62O6Si

Base Information
  • Chemical Name:C35H62O6Si
  • CAS No.:1003890-47-8
  • Molecular Formula:C35H62O6Si
  • Molecular Weight:606.959
  • Hs Code.:
C<sub>35</sub>H<sub>62</sub>O<sub>6</sub>Si

Synonyms:C35H62O6Si

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Chemical Property of C35H62O6Si
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Technology Process of C35H62O6Si

There total 9 articles about C35H62O6Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
4-iodo-2-methyl-but-1-ene; With magnesium; In diethyl ether; Heating;
C30H52O6Si; In diethyl ether; at -78 - 20 ℃; Further stages.;
DOI:10.1021/ol7025944
Guidance literature:
Multi-step reaction with 7 steps
1.1: Hoveyda-Grubbs catalyst second generation / 1,1-dichloroethane / 90 °C / Inert atmosphere
2.1: 2-nitrobenzenesulfonyl hydrazide; triethylamine / 1,2-dichloro-ethane / Inert atmosphere
3.1: formic acid; palladium diacetate; triethylamine / 1,2-dichloro-ethane / 40 °C / Inert atmosphere
3.2: Inert atmosphere
4.1: lithium aluminium tetrahydride / diethyl ether / Inert atmosphere
5.1: pyridinium p-toluenesulfonate / dichloromethane / Inert atmosphere
6.1: pyridine; ozone / methanol; dichloromethane / -78 °C / Inert atmosphere
6.2: Inert atmosphere
7.1: magnesium / diethyl ether / -78 °C / Inert atmosphere
With pyridine; lithium aluminium tetrahydride; formic acid; Hoveyda-Grubbs catalyst second generation; 2-nitrobenzenesulfonyl hydrazide; palladium diacetate; pyridinium p-toluenesulfonate; ozone; magnesium; triethylamine; In methanol; diethyl ether; 1,1-dichloroethane; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jo2003506
Guidance literature:
Multi-step reaction with 8 steps
1.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane
2.1: Hoveyda-Grubbs catalyst second generation / 1,1-dichloroethane / 90 °C / Inert atmosphere
3.1: 2-nitrobenzenesulfonyl hydrazide; triethylamine / 1,2-dichloro-ethane / Inert atmosphere
4.1: formic acid; palladium diacetate; triethylamine / 1,2-dichloro-ethane / 40 °C / Inert atmosphere
4.2: Inert atmosphere
5.1: lithium aluminium tetrahydride / diethyl ether / Inert atmosphere
6.1: pyridinium p-toluenesulfonate / dichloromethane / Inert atmosphere
7.1: pyridine; ozone / methanol; dichloromethane / -78 °C / Inert atmosphere
7.2: Inert atmosphere
8.1: magnesium / diethyl ether / -78 °C / Inert atmosphere
With pyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; lithium aluminium tetrahydride; formic acid; Hoveyda-Grubbs catalyst second generation; 2-nitrobenzenesulfonyl hydrazide; palladium diacetate; pyridinium p-toluenesulfonate; ozone; magnesium; triethylamine; In methanol; diethyl ether; 1,1-dichloroethane; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jo2003506
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