N-[2-N-(N-(tert-butyloxycarbonyl)-L-phenylalanyl)amino-DL-dodecanoyl]-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylamine

Base Information

• Chemical Name: N-[2-N-(N-(tert-butyloxycarbonyl)-L-phenylalanyl)amino-DL-dodecanoyl]-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylamine
• CAS No.: 1198790-32-7
• Molecular Formula: C₄₀H₆₁N₃O₁₃
• Molecular Weight: 791.937

Synonyms:N-[2-N-(N-(tert-butyloxycarbonyl)-L-phenylalanyl)amino-DL-dodecanoyl]-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylamine

Chemical Property of N-[2-N-(N-(tert-butyloxycarbonyl)-L-phenylalanyl)amino-DL-dodecanoyl]-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylamine

Chemical Property:

Purity/Quality:

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Technology Process of N-[2-N-(N-(tert-butyloxycarbonyl)-L-phenylalanyl)amino-DL-dodecanoyl]-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylamine

There total 1 articles about N-[2-N-(N-(tert-butyloxycarbonyl)-L-phenylalanyl)amino-DL-dodecanoyl]-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

N-(2-amino-DL-dodecanoyl)-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylamine (293751-98-1) + N-tert-butoxycarbonyl-L-phenylalanine (13734-34-4) → N-[2-N-(N-(tert-butyloxycarbonyl)-L-phenylalanyl)amino-DL-dodecanoyl]-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylamine (1198790-32-7)

Guidance literature:

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; at 20 ℃; for 12h;

DOI:10.1016/j.tet.2009.08.072

Reference yield: 95.0%

N-[2-N-(N-(tert-butyloxycarbonyl)-L-phenylalanyl)amino-DL-dodecanoyl]-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylamine (1198790-32-7) → N-[2-(N'-L-phenylalanyl)amino-DL-dodecanoyl]-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylamine (1198790-35-0)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 1h;

DOI:10.1016/j.tet.2009.08.072

upstream raw materials:

N-(2-amino-DL-dodecanoyl)-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylamine

N-tert-butoxycarbonyl-L-phenylalanine

Downstream raw materials:

N-[2-(N'-L-phenylalanyl)amino-DL-dodecanoyl]-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylamine

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