N-[4-[(E)-2-(4,4,6-trimethyl-1,3,2-dioxaborinan-2-yl)vinyl]phenyl]methanesulfonamide

Base Information

Chemical Name:N-[4-[(E)-2-(4,4,6-trimethyl-1,3,2-dioxaborinan-2-yl)vinyl]phenyl]methanesulfonamide
CAS No.:1206775-11-2
Molecular Formula:C₁₅H₂₂BNO₄S
Molecular Weight:323.221
Hs Code.:

Synonyms:N-[4-[(E)-2-(4,4,6-trimethyl-1,3,2-dioxaborinan-2-yl)vinyl]phenyl]methanesulfonamide

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Chemical Property of N-[4-[(E)-2-(4,4,6-trimethyl-1,3,2-dioxaborinan-2-yl)vinyl]phenyl]methanesulfonamide

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Technology Process of N-[4-[(E)-2-(4,4,6-trimethyl-1,3,2-dioxaborinan-2-yl)vinyl]phenyl]methanesulfonamide

There total 1 articles about N-[4-[(E)-2-(4,4,6-trimethyl-1,3,2-dioxaborinan-2-yl)vinyl]phenyl]methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 102294-59-7
N-(4-iodophenyl)-methanesulfonamide

: 4627-10-5
4,4,6-trimethyl-2-vinyl-1,3,2-dioxaborinane

: 1206775-11-2
N-[4-[(E)-2-(4,4,6-trimethyl-1,3,2-dioxaborinan-2-yl)vinyl]phenyl]methanesulfonamide

Guidance literature:: With tributyl-amine; palladium diacetate; tris-(o-tolyl)phosphine; In toluene; for 72h; under 760.051 Torr; Inert atmosphere; Reflux;

Reference yield: 64.0%

: 1206775-11-2
N-[4-[(E)-2-(4,4,6-trimethyl-1,3,2-dioxaborinan-2-yl)vinyl]phenyl]methanesulfonamide

: 3-[3-bromo-4-methoxy-5-(3-methyloxetan-3-yl)phenyl]-1H-pyridin-2-one

: 1206773-88-7
N-[4-[(E)-2-[2-methoxy-3-(3-methyloxetan-3-yl)-5-(2-oxo-1H-pyridin-3-yl)phenyl]vinyl]phenyl]methanesulfonamide

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In methanol; dichloromethane; at 120 ℃; for 1h; Inert atmosphere; Microwave irradiation;
DOI:10.1021/jm401266k

Reference yield: 41.0%

: 1044771-51-8
2-tert-butyl-4,6-dichloropyrimidine

: 1206775-11-2
N-[4-[(E)-2-(4,4,6-trimethyl-1,3,2-dioxaborinan-2-yl)vinyl]phenyl]methanesulfonamide

: C₁₇H₂₀ClN₃O₂S

Guidance literature:: With potassium phosphate monohydrate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 100 ℃; for 6h; Sealed tube;