ethyl 5-<3-<<(dimethylethyl)diphenylsilyl>oxy>propyl>-3-isoxazolecarboxylate

Base Information

Chemical Name:ethyl 5-<3-<<(dimethylethyl)diphenylsilyl>oxy>propyl>-3-isoxazolecarboxylate
CAS No.:156787-22-3
Molecular Formula:C₂₅H₃₁NO₄Si
Molecular Weight:437.611
Hs Code.:

Synonyms:ethyl 5-<3-<<(dimethylethyl)diphenylsilyl>oxy>propyl>-3-isoxazolecarboxylate

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Chemical Property of ethyl 5-<3-<<(dimethylethyl)diphenylsilyl>oxy>propyl>-3-isoxazolecarboxylate

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Technology Process of ethyl 5-<3-<<(dimethylethyl)diphenylsilyl>oxy>propyl>-3-isoxazolecarboxylate

There total 4 articles about ethyl 5-<3-<<(dimethylethyl)diphenylsilyl>oxy>propyl>-3-isoxazolecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.6%

: 95080-93-6
ethyl chlorooximidoacetate

: 91266-03-4
tert-butyl-pent-4-ynyloxy-diphenyl-silane

: 156787-22-3
ethyl 5-<3-<<(dimethylethyl)diphenylsilyl>oxy>propyl>-3-isoxazolecarboxylate

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; for 3.5h;
DOI:10.1021/jm00041a022

Reference yield:

: 5390-04-5
pent-1-yn-5-ol

: 156787-22-3
ethyl 5-<3-<<(dimethylethyl)diphenylsilyl>oxy>propyl>-3-isoxazolecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 86.8 percent / imidazole / dimethylformamide / 2 h / Ambient temperature

2: 76.6 percent / Et₃N / dimethylformamide / 3.5 h

With 1H-imidazole; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/jm00041a022

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 156787-22-3
ethyl 5-<3-<<(dimethylethyl)diphenylsilyl>oxy>propyl>-3-isoxazolecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 86.8 percent / imidazole / dimethylformamide / 2 h / Ambient temperature

2: 76.6 percent / Et₃N / dimethylformamide / 3.5 h

With 1H-imidazole; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/jm00041a022