2'-hydroxy-4'-<(β-methoxyethoxy)methoxy>-6'-methyl-2-(methylsulfinyl)acetophenone

Base Information

Chemical Name:2'-hydroxy-4'-<(β-methoxyethoxy)methoxy>-6'-methyl-2-(methylsulfinyl)acetophenone
CAS No.:104783-90-6
Molecular Formula:C₁₄H₂₀O₆S
Molecular Weight:316.375
Hs Code.:

Synonyms:2'-hydroxy-4'-<(β-methoxyethoxy)methoxy>-6'-methyl-2-(methylsulfinyl)acetophenone

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Chemical Property of 2'-hydroxy-4'-<(β-methoxyethoxy)methoxy>-6'-methyl-2-(methylsulfinyl)acetophenone

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Technology Process of 2'-hydroxy-4'-<(β-methoxyethoxy)methoxy>-6'-methyl-2-(methylsulfinyl)acetophenone

There total 3 articles about 2'-hydroxy-4'-<(β-methoxyethoxy)methoxy>-6'-methyl-2-(methylsulfinyl)acetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2524-37-0
ethyl orselinate

: 104783-90-6
2'-hydroxy-4'-<(β-methoxyethoxy)methoxy>-6'-methyl-2-(methylsulfinyl)acetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / triethylamine / CH₂Cl₂ / 48 h / Ambient temperature

2: 1.) sodium hydride / 1.) benzene, 80 deg C, 1 h, 2.) benzene, a) 35 deg C, b) 45 to 50 deg C, 1 h

With sodium hydride; triethylamine; In dichloromethane;

Reference yield:

: 21855-46-9
ethyl 3,5-dibromo-2,4-dihydroxy-6-methyl benzoate

: 104783-90-6
2'-hydroxy-4'-<(β-methoxyethoxy)methoxy>-6'-methyl-2-(methylsulfinyl)acetophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / H₂ / 10percent Pd/C / aq. NaOH / 15 h / 760 Torr / Ambient temperature

2: 60 percent / triethylamine / CH₂Cl₂ / 48 h / Ambient temperature

3: 1.) sodium hydride / 1.) benzene, 80 deg C, 1 h, 2.) benzene, a) 35 deg C, b) 45 to 50 deg C, 1 h

With hydrogen; sodium hydride; triethylamine; palladium on activated charcoal; In sodium hydroxide; dichloromethane;

Reference yield:

: 67-68-5,8070-53-9
dimethyl sulfoxide

: ethyl 2-hydroxy-4-<(β-methoxyethoxy)methoxy>-6-methylbenzoate

: 104783-90-6
2'-hydroxy-4'-<(β-methoxyethoxy)methoxy>-6'-methyl-2-(methylsulfinyl)acetophenone

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) benzene, 80 deg C, 1 h, 2.) benzene, a) 35 deg C, b) 45 to 50 deg C, 1 h;