bis(bromo-tert-butylboryl)phenylamine

Base Information

Chemical Name:bis(bromo-tert-butylboryl)phenylamine
CAS No.:137517-07-8
Molecular Formula:C₁₄H₂₃B₂Br₂N
Molecular Weight:386.773
Hs Code.:

Synonyms:bis(bromo-tert-butylboryl)phenylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(bromo-tert-butylboryl)phenylamine

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of bis(bromo-tert-butylboryl)phenylamine

There total 2 articles about bis(bromo-tert-butylboryl)phenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 2767-47-7
dimethyltin dibromide

: 17729-33-8
N,N-bis(trimethylstannyl)phenylamine

: 106192-86-3
dibromo-tert-butylborane

: 1066-44-0
trimethyltin bromide

: 137517-07-8
bis(bromo-tert-butylboryl)phenylamine

Guidance literature:: In dichloromethane; N2 atmosphere, addn. of soln. of stannyl compound to suspension of Me2SnBr2 at room temp., addn. of soln. of tBuBBr2 at -68 to -40°C (130min), warming to room temp.; removement of solvent (25°C, 12 Torr), condensation of Me3SnBr and Me2SnBr2 into a trap (-78°C, 4 h), fractional distillation (69-77°C, 1E-5 Torr); elem. anal.;

Reference yield: 69.0%

: 17729-33-8
N,N-bis(trimethylstannyl)phenylamine

: 106192-86-3
dibromo-tert-butylborane

: 137517-07-8
bis(bromo-tert-butylboryl)phenylamine

Guidance literature:: N,N-bis(trimethylstannyl)phenylamine; With dimethyltin dibromide; In dichloromethane; at 20 ℃;

dibromo-tert-butylborane; In dichloromethane; at -40 - 20 ℃;