C₂₆H₃₄O₄S

Base Information

Chemical Name:C₂₆H₃₄O₄S
CAS No.:76685-63-7
Molecular Formula:C₂₆H₃₄O₄S
Molecular Weight:442.62
Hs Code.:

C<sub>26</sub>H<sub>34</sub>O<sub>4</sub>S

Synonyms:C₂₆H₃₄O₄S

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Chemical Property of C₂₆H₃₄O₄S

Chemical Property:

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Technology Process of C₂₆H₃₄O₄S

There total 14 articles about C₂₆H₃₄O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76685-62-6
C₂₉H₄₀O₃S₃

: 76685-63-7
C₂₆H₃₄O₄S

Guidance literature:: With 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; In tetrahydrofuran; water; acetone; at -20 ℃; for 0.5h;
DOI:10.1021/ja00545a060

Reference yield:

: 76685-50-2
(4aS,8aS)-5,5,8a-Trimethyl-2-oxo-1,2,3,4,4a,5,8,8a-octahydro-naphthalene-1-carbaldehyde

: 76685-63-7
C₂₆H₃₄O₄S

Guidance literature:: Multi-step reaction with 9 steps

1: 70 percent / 1,5-diazabicyclo<5.4.0>undec-5-ene, potassium carbonate / tetrahydrofuran; 2-methyl-propan-2-ol / 23 °C

2: 93 percent / pyrrolidinium acetate / tetrahydrofuran; methanol / 23 °C

3: zinc iodide / CHCl₃ / 23 °C

4: 87 percent

5: 80 percent / diisobutylaluminum hydride / toluene / -10 - -5 °C

6: 1.) trimethylsilyllithium, 2.) lithium diisopropylamide / 1.) ether, HMPA, -35 deg C, 2.) THF, HMPA, 23 deg C

7: sodium borohydride / tetrahydrofuran; ethanol / 0 °C

8: 4-(dimethylamino)pyridine / pyridine; CHCl₃ / 23 °C

9: 1,3-diiodo-5,5-dimethylhydantoin / acetone; tetrahydrofuran; H₂O / 0.5 h / -20 °C

With trimethylsilyl lithium; dmap; sodium tetrahydroborate; 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; diisobutylaluminium hydride; pyrrolidine acetic acid; potassium carbonate; zinc(II) iodide; 1,5-Diazabicyclo[5.4.0]undec-5-ene; lithium diisopropyl amide; In tetrahydrofuran; pyridine; methanol; ethanol; chloroform; water; acetone; toluene; tert-butyl alcohol;
DOI:10.1021/ja00545a060

Reference yield:

: 76685-52-4
((4'aR,8'aR)-5',5',8'a-Trimethyl-3',4',4'a,5',8',8'a-hexahydro-1'H-spiro[[1,3]dioxolane-2,2'-naphthalen]-1'-yl)-methanol

: 76685-63-7
C₂₆H₃₄O₄S

Guidance literature:: Multi-step reaction with 11 steps

1: 92 percent / pyridinium chlorochromate / CH₂Cl₂ / 23 °C

2: 96 percent / aq. perchloric acid / acetone / 3 h / 23 °C

3: 70 percent / 1,5-diazabicyclo<5.4.0>undec-5-ene, potassium carbonate / tetrahydrofuran; 2-methyl-propan-2-ol / 23 °C

4: 93 percent / pyrrolidinium acetate / tetrahydrofuran; methanol / 23 °C

5: zinc iodide / CHCl₃ / 23 °C

6: 87 percent

7: 80 percent / diisobutylaluminum hydride / toluene / -10 - -5 °C

8: 1.) trimethylsilyllithium, 2.) lithium diisopropylamide / 1.) ether, HMPA, -35 deg C, 2.) THF, HMPA, 23 deg C

9: sodium borohydride / tetrahydrofuran; ethanol / 0 °C

10: 4-(dimethylamino)pyridine / pyridine; CHCl₃ / 23 °C

11: 1,3-diiodo-5,5-dimethylhydantoin / acetone; tetrahydrofuran; H₂O / 0.5 h / -20 °C

With trimethylsilyl lithium; dmap; sodium tetrahydroborate; perchloric acid; 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; diisobutylaluminium hydride; pyrrolidine acetic acid; potassium carbonate; pyridinium chlorochromate; zinc(II) iodide; 1,5-Diazabicyclo[5.4.0]undec-5-ene; lithium diisopropyl amide; In tetrahydrofuran; pyridine; methanol; ethanol; dichloromethane; chloroform; water; acetone; toluene; tert-butyl alcohol;
DOI:10.1021/ja00545a060