C₂₈H₄₂O₄S₃Si

Base Information

Chemical Name:C₂₈H₄₂O₄S₃Si
CAS No.:1377314-00-5
Molecular Formula:C₂₈H₄₂O₄S₃Si
Molecular Weight:566.923
Hs Code.:

C<sub>28</sub>H<sub>42</sub>O<sub>4</sub>S<sub>3</sub>Si

Synonyms:C₂₈H₄₂O₄S₃Si

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Chemical Property of C₂₈H₄₂O₄S₃Si

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Technology Process of C₂₈H₄₂O₄S₃Si

There total 6 articles about C₂₈H₄₂O₄S₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1377313-97-7
C₂₈H₄₂O₄S₃Si

: 1377314-00-5
C₂₈H₄₂O₄S₃Si

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In toluene; at 85 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol301144a

Reference yield:

: 14947-48-9
2-(2'-hydroxyethyl)-1,3-dithiane

: 1377314-00-5
C₂₈H₄₂O₄S₃Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 1 h / 0 - 20 °C / Inert atmosphere

2.1: barium(II) hydroxide / tetrahydrofuran; water / 0.5 h / Inert atmosphere

2.2: 1 h / 0 °C / Inert atmosphere

3.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / tetrahydrofuran; methanol / 0.5 h / 0 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

4.2: 1 h / -78 °C / Inert atmosphere

5.1: Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

6.1: 18-crown-6 ether; potassium carbonate / toluene / 1 h / 85 °C / Inert atmosphere

With sodium tetrahydroborate; n-butyllithium; 18-crown-6 ether; cerium(III) chloride heptahydrate; sulfur trioxide pyridine complex; potassium carbonate; Dess-Martin periodane; triethylamine; barium(II) hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; toluene; 6.1: Michael addition;
DOI:10.1021/ol301144a

Reference yield:

: C₂₈H₄₄O₄S₃Si

: 1377314-00-5
C₂₈H₄₂O₄S₃Si

Guidance literature:: Multi-step reaction with 2 steps

1: Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

2: 18-crown-6 ether; potassium carbonate / toluene / 1 h / 85 °C / Inert atmosphere

With 18-crown-6 ether; potassium carbonate; Dess-Martin periodane; In dichloromethane; toluene; 2: Michael addition;
DOI:10.1021/ol301144a