(1,2-bis[N,N'-{p-nitrobenzyl}methyl]-N,N'-[6-{methoxycarbonyl}-pyridin-2-yl]methylamino)ethane

Base Information

Chemical Name:(1,2-bis[N,N'-{p-nitrobenzyl}methyl]-N,N'-[6-{methoxycarbonyl}-pyridin-2-yl]methylamino)ethane
CAS No.:1255535-31-9
Molecular Formula:C₃₂H₃₂N₆O₈
Molecular Weight:628.641
Hs Code.:

Synonyms:(1,2-bis[N,N'-{p-nitrobenzyl}methyl]-N,N'-[6-{methoxycarbonyl}-pyridin-2-yl]methylamino)ethane

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Chemical Property of (1,2-bis[N,N'-{p-nitrobenzyl}methyl]-N,N'-[6-{methoxycarbonyl}-pyridin-2-yl]methylamino)ethane

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Technology Process of (1,2-bis[N,N'-{p-nitrobenzyl}methyl]-N,N'-[6-{methoxycarbonyl}-pyridin-2-yl]methylamino)ethane

There total 1 articles about (1,2-bis[N,N'-{p-nitrobenzyl}methyl]-N,N'-[6-{methoxycarbonyl}-pyridin-2-yl]methylamino)ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 761411-41-0
dimethyl 6,6′-([ethane-1,2-diylbis{azanediyl}]bis[methylene])dipicolinate

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 1255535-31-9
(1,2-bis[N,N'-{p-nitrobenzyl}methyl]-N,N'-[6-{methoxycarbonyl}-pyridin-2-yl]methylamino)ethane

Guidance literature:: With sodium carbonate; In acetonitrile; at 70 ℃;
DOI:10.1021/ja106399h

Reference yield: 97.0%

: 1255535-31-9
(1,2-bis[N,N'-{p-nitrobenzyl}methyl]-N,N'-[6-{methoxycarbonyl}-pyridin-2-yl]methylamino)ethane

: 1255535-32-0
1,2-bis[N,N'-{p-nitrobenzyl}methyl]-N,N'-bis-[6-carboxy-2-pyridylmethyl]ethylenediamine

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; for 0.75h;
DOI:10.1021/ja106399h

Reference yield:

: 1255535-31-9
(1,2-bis[N,N'-{p-nitrobenzyl}methyl]-N,N'-[6-{methoxycarbonyl}-pyridin-2-yl]methylamino)ethane

: C₃₀H₂₈GaN₆O₈⁽¹⁺⁾*NO₃^(1-)

Guidance literature:: Multi-step reaction with 2 steps

1: water; lithium hydroxide / tetrahydrofuran / 0.75 h

2: sodium hydroxide / water; methanol / 2 h / 60 °C / pH 4.5

With water; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; water;