2-((2S,3R,4R,6R)-4-Allyloxy-6-benzyloxymethyl-2-ethylsulfanyl-5-oxo-tetrahydro-pyran-3-yl)-isoindole-1,3-dione

Base Information

Chemical Name:2-((2S,3R,4R,6R)-4-Allyloxy-6-benzyloxymethyl-2-ethylsulfanyl-5-oxo-tetrahydro-pyran-3-yl)-isoindole-1,3-dione
CAS No.:860640-11-5
Molecular Formula:C₂₆H₂₇NO₆S
Molecular Weight:481.569
Hs Code.:

Synonyms:2-((2S,3R,4R,6R)-4-Allyloxy-6-benzyloxymethyl-2-ethylsulfanyl-5-oxo-tetrahydro-pyran-3-yl)-isoindole-1,3-dione

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Chemical Property of 2-((2S,3R,4R,6R)-4-Allyloxy-6-benzyloxymethyl-2-ethylsulfanyl-5-oxo-tetrahydro-pyran-3-yl)-isoindole-1,3-dione

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Technology Process of 2-((2S,3R,4R,6R)-4-Allyloxy-6-benzyloxymethyl-2-ethylsulfanyl-5-oxo-tetrahydro-pyran-3-yl)-isoindole-1,3-dione

There total 3 articles about 2-((2S,3R,4R,6R)-4-Allyloxy-6-benzyloxymethyl-2-ethylsulfanyl-5-oxo-tetrahydro-pyran-3-yl)-isoindole-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 419549-63-6
ethyl 3-O-allyl-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 860640-11-5
2-((2S,3R,4R,6R)-4-Allyloxy-6-benzyloxymethyl-2-ethylsulfanyl-5-oxo-tetrahydro-pyran-3-yl)-isoindole-1,3-dione

Guidance literature:: With pyridine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; dimethyl sulfoxide;
DOI:10.1081/CAR-200061584

Reference yield:

: ethyl 3-O-allyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 860640-11-5
2-((2S,3R,4R,6R)-4-Allyloxy-6-benzyloxymethyl-2-ethylsulfanyl-5-oxo-tetrahydro-pyran-3-yl)-isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / sodium cyanoborohydride; molecular sieves 3 Angstroem; HCl / tetrahydrofuran; diethyl ether / 2 h / 0 °C

2: N,N'-dicyclohexylcarbodiimide; pyridine; trifluoroacetic acid / CH₂Cl₂; dimethylsulfoxide

With pyridine; hydrogenchloride; 3 A molecular sieve; sodium cyanoborohydride; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1081/CAR-200061584

Reference yield:

: 99409-33-3
ethyl 4,6-O-benzylidene-2-deoxy-2-N-phthalamido-1-thio-β-Dglucopyranoside

: 860640-11-5
2-((2S,3R,4R,6R)-4-Allyloxy-6-benzyloxymethyl-2-ethylsulfanyl-5-oxo-tetrahydro-pyran-3-yl)-isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / NaH / dimethylformamide; various solvent(s) / 2 h / 0 °C

2: 82 percent / sodium cyanoborohydride; molecular sieves 3 Angstroem; HCl / tetrahydrofuran; diethyl ether / 2 h / 0 °C

3: N,N'-dicyclohexylcarbodiimide; pyridine; trifluoroacetic acid / CH₂Cl₂; dimethylsulfoxide

With pyridine; hydrogenchloride; 3 A molecular sieve; sodium hydride; sodium cyanoborohydride; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1081/CAR-200061584