4-(4-(2-(5-isopropyl-2,4-bis((4-methoxybenzyl)oxy)phenyl)-5-(pyridin-3-yl)-1H-pyrrol-1-yl)phenyl)morpholine

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Chemical Name:4-(4-(2-(5-isopropyl-2,4-bis((4-methoxybenzyl)oxy)phenyl)-5-(pyridin-3-yl)-1H-pyrrol-1-yl)phenyl)morpholine
CAS No.:1465044-67-0
Molecular Formula:C₄₄H₄₅N₃O₅
Molecular Weight:695.858
Hs Code.:

Synonyms:4-(4-(2-(5-isopropyl-2,4-bis((4-methoxybenzyl)oxy)phenyl)-5-(pyridin-3-yl)-1H-pyrrol-1-yl)phenyl)morpholine

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Chemical Property of 4-(4-(2-(5-isopropyl-2,4-bis((4-methoxybenzyl)oxy)phenyl)-5-(pyridin-3-yl)-1H-pyrrol-1-yl)phenyl)morpholine

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Technology Process of 4-(4-(2-(5-isopropyl-2,4-bis((4-methoxybenzyl)oxy)phenyl)-5-(pyridin-3-yl)-1H-pyrrol-1-yl)phenyl)morpholine

There total 6 articles about 4-(4-(2-(5-isopropyl-2,4-bis((4-methoxybenzyl)oxy)phenyl)-5-(pyridin-3-yl)-1H-pyrrol-1-yl)phenyl)morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.6%

: 2524-67-6,86759-37-7
4-morpholino-4-yl-phenylamine

: 1465044-65-8
1-(5-isopropyl-2,4-bis((4-methoxybenzyl)oxy)phenyl)-4-(pyridin-3-yl)butane-1,4-dione

: 1465044-67-0
4-(4-(2-(5-isopropyl-2,4-bis((4-methoxybenzyl)oxy)phenyl)-5-(pyridin-3-yl)-1H-pyrrol-1-yl)phenyl)morpholine

Guidance literature:: With toluene-4-sulfonic acid; In ethanol; at 110 ℃; for 2h; Microwave irradiation;

Reference yield:

: 1465044-62-5
1-(5-isopropyl-2,4-bis((4-methoxybenzyl)oxy)phenyl)prop-2-en-1-one

: 1465044-67-0
4-(4-(2-(5-isopropyl-2,4-bis((4-methoxybenzyl)oxy)phenyl)-5-(pyridin-3-yl)-1H-pyrrol-1-yl)phenyl)morpholine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide / 1 h / 70 °C / Inert atmosphere; Microwave irradiation

2: toluene-4-sulfonic acid / ethanol / 2 h / 110 °C / Microwave irradiation

With 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; toluene-4-sulfonic acid; triethylamine; In ethanol;

Reference yield:

: 958888-27-2
5-isopropyl-2,4-dihydroxy benzaldehyde

: 1465044-67-0
4-(4-(2-(5-isopropyl-2,4-bis((4-methoxybenzyl)oxy)phenyl)-5-(pyridin-3-yl)-1H-pyrrol-1-yl)phenyl)morpholine

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate; N,N-dimethyl-formamide / 3 h / 60 °C

2: tetrahydrofuran / -5 - 20 °C

3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 20 °C

4: triethylamine; 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide / 1 h / 70 °C / Inert atmosphere; Microwave irradiation

5: toluene-4-sulfonic acid / ethanol / 2 h / 110 °C / Microwave irradiation

With 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; potassium carbonate; toluene-4-sulfonic acid; triethylamine; N,N-dimethyl-formamide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; ethanol; dichloromethane;