(1R,3R)-3-methylcyclopentadecyl acetate

Base Information

• Chemical Name: (1R,3R)-3-methylcyclopentadecyl acetate
• CAS No.: 504414-47-5
• Molecular Formula: C₁₈H₃₄O₂
• Molecular Weight: 282.467
• Mol file: 504414-47-5.mol

Synonyms:(1R,3R)-3-methylcyclopentadecyl acetate

Chemical Property of (1R,3R)-3-methylcyclopentadecyl acetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1R,3R)-3-methylcyclopentadecyl acetate

There total 1 articles about (1R,3R)-3-methylcyclopentadecyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

(1RS,3RS)-3-methylcyclopentadecanol + vinyl acetate (108-05-4,9003-20-7) → (1R,3R)-3-methylcyclopentadecyl acetate (504414-47-5) + 3-methylcyclopentadecan-1-ol (62151-56-8)

Guidance literature:

With lipase QLG; In tetrahydrofuran; at 20 ℃; for 24h;

DOI:10.1002/hlca.200790101

Reference yield:

(1R,3R)-3-methylcyclopentadecyl acetate (504414-47-5) → (R)-3-methyl-1-cyclopentadecanone (10403-00-6,22460-48-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 92 percent / KOH / methanol / 17 h / 20 °C

2: 81 percent / pyridinium dichromate / CH₂Cl₂ / 48 h / 20 °C

With potassium hydroxide; dipyridinium dichromate; In methanol; dichloromethane;

DOI:10.1002/hlca.200790101

Reference yield:

(1R,3R)-3-methylcyclopentadecyl acetate (504414-47-5) → 2-[(1R,3R)-3-methylcyclopentadecyl] hydrogen 3-nitrobenzene-1,2-dicarboxylate

Guidance literature:

Multi-step reaction with 2 steps

1: 92 percent / KOH / methanol / 17 h / 20 °C

2: 86 percent / toluene / 2 h / Heating

With potassium hydroxide; In methanol; toluene;

DOI:10.1002/hlca.200790101

upstream raw materials:

vinyl acetate

Downstream raw materials:

(1S,3R)-3-methylcyclopentadecyl benzoate

(R)-3-methyl-1-cyclopentadecanone

Refernces