[(4-methoxyphenyl)sulfonyl]carbonochloridimidothioic acid methyl ester

Base Information

• Chemical Name: [(4-methoxyphenyl)sulfonyl]carbonochloridimidothioic acid methyl ester
• CAS No.: 127611-21-6
• Molecular Formula: C₉H₁₀ClNO₃S₂
• Molecular Weight: 279.768

Synonyms:[(4-methoxyphenyl)sulfonyl]carbonochloridimidothioic acid methyl ester

Chemical Property of [(4-methoxyphenyl)sulfonyl]carbonochloridimidothioic acid methyl ester

Chemical Property:

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Technology Process of [(4-methoxyphenyl)sulfonyl]carbonochloridimidothioic acid methyl ester

There total 1 articles about [(4-methoxyphenyl)sulfonyl]carbonochloridimidothioic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

[(4-methoxyphenyl)sulfonyl]carbonimidodithioic acid dimethyl ester (93420-43-0) → [(4-methoxyphenyl)sulfonyl]carbonochloridimidothioic acid methyl ester (127611-21-6)

Guidance literature:

With sulfuryl dichloride; In dichloromethane; at 40 ℃; for 3h;

DOI:10.1021/ja071501o

Reference yield:

(4R,5S)-4-((Z)-4-Amino-but-1-enyl)-3-(4-methoxy-benzyl)-2,2-dioxo-2λ6-[1,2,3]oxathiazinan-5-ol + [(4-methoxyphenyl)sulfonyl]carbonochloridimidothioic acid methyl ester (127611-21-6) → N-[1-{(Z)-4-[(4R,5S)-5-Hydroxy-3-(4-methoxy-benzyl)-2,2-dioxo-2λ6-[1,2,3]oxathiazinan-4-yl]-but-3-enylamino}-1-methylsulfanyl-meth-(Z)-ylidene]-4-methoxy-benzenesulfonamide (884335-19-7)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In acetonitrile;

DOI:10.1021/ja0608545

Reference yield:

C31H51N7O10 + [(4-methoxyphenyl)sulfonyl]carbonochloridimidothioic acid methyl ester (127611-21-6) → C40H60N8O13S2

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 24h; Inert atmosphere;

DOI:10.1039/c3ob41398e

upstream raw materials:

[(4-methoxyphenyl)sulfonyl]carbonimidodithioic acid dimethyl ester

Downstream raw materials:

N-[1-{(Z)-4-[(4R,5S)-5-Hydroxy-3-(4-methoxy-benzyl)-2,2-dioxo-2λ⁶-[1,2,3]oxathiazinan-4-yl]-but-3-enylamino}-1-methylsulfanyl-meth-(Z)-ylidene]-4-methoxy-benzenesulfonamide

C₂₄H₃₀N₄O₆S₂

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