C₃₀H₃₅NO₃

Base Information

Chemical Name:C₃₀H₃₅NO₃
CAS No.:124665-47-0
Molecular Formula:C₃₀H₃₅NO₃
Molecular Weight:457.613
Hs Code.:

C<sub>30</sub>H<sub>35</sub>NO<sub>3</sub>

Synonyms:C₃₀H₃₅NO₃

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Chemical Property of C₃₀H₃₅NO₃

Chemical Property:

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Technology Process of C₃₀H₃₅NO₃

There total 27 articles about C₃₀H₃₅NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 124665-44-7
C₃₁H₃₇NO₃

: 124665-48-1
C₂₃H₂₉NO₂

: 124665-47-0
C₃₀H₃₅NO₃

Guidance literature:: With sodium hydride; ethanethiol; In N,N-dimethyl-formamide; at 150 ℃; for 1h;
DOI:10.1016/S0040-4020(01)83440-2

Reference yield:

: 124665-51-6
2-((1R,2S,6S,7S)-2-Benzyloxymethyl-5,5-dimethoxy-bicyclo[4.2.0]oct-7-yl)-propan-2-ol

: 124665-47-0
C₃₀H₃₅NO₃

Guidance literature:: Multi-step reaction with 18 steps

1: pyridinium p-toluenesulfonate / acetone / 0.33 h / Ambient temperature

2: 84 percent / N-ethyldiisopropylamine / CH₂Cl₂ / 46 h / Ambient temperature

3: sodium hydride / tetrahydrofuran / 6.5 h / Ambient temperature

4: triethylamine / 1.) 0 deg C, 1h; 2.) rt, 36h

5: potassium hydroxide / methanol; H₂O / 2.5 h / Heating

6: 87 percent / hydroxylamine hydrochloride, sodium acetate / methanol / 0.67 h / Heating

7: xylene / 0.83 h / 150 °C

8: sodium hydroxide / ethanol; H₂O / 7.25 h / Heating

9: 84 percent / H₂, (1S)-(+)-10-camphorsulfonic acid / palladium hydroxide on carbon / ethyl acetate / 22.5 h

10: 85 percent / N-ethyldiisopropylamine / 4-dimethylaminopyridine / CH₂Cl₂ / 1.) 0 deg C, 40 min; 2.) rt,1.33 h

11: lithium diisopropylamide / hexane; tetrahydrofuran / 1.) 0 deg C, 50 min; 2.) rt, 50 min

12: 83 percent / n-BuLi / hexane; tetrahydrofuran / 1.1 h / Ambient temperature

13: pyridinium p-toluenesulfonate / dimethylformamide / 0.83 h / Ambient temperature

14: sodium hydride / dimethylformamide / 1.25 h

15: 99 percent / acetic acid; tetrahydrofuran; propan-2-ol / 8.5 h / Ambient temperature

16: 88 percent / dicyclohexylcarbodiimide, pyridine, trifluoroacetic acid, DMSO / benzene / 4.5 h / Ambient temperature

17: 61 percent / (1S)-(+)-10-camphorsulfonic acid / methanol; toluene / 3 h / Ambient temperature

18: 65 percent / ethanethiol, sodium hydride / dimethylformamide / 1 h / 150 °C

With pyridine; potassium hydroxide; sodium hydroxide; n-butyllithium; hydroxylamine hydrochloride; hydrogen; sodium acetate; pyridinium p-toluenesulfonate; sodium hydride; dimethyl sulfoxide; (+)-10-camphorsulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; ethanethiol; lithium diisopropyl amide; dmap; palladium dihydroxide; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; acetic acid; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol; acetone; toluene; xylene; benzene;
DOI:10.1016/S0040-4020(01)83440-2

Reference yield:

: 124665-55-0
(1S,5S,6R,8S)-5-Benzyloxymethyl-3-[1-hydroxy-meth-(Z)-ylidene]-8-(1-methoxymethoxy-1-methyl-ethyl)-bicyclo[4.2.0]octan-2-one

: 124665-47-0
C₃₀H₃₅NO₃

Guidance literature:: Multi-step reaction with 15 steps

1: triethylamine / 1.) 0 deg C, 1h; 2.) rt, 36h

2: potassium hydroxide / methanol; H₂O / 2.5 h / Heating

3: 87 percent / hydroxylamine hydrochloride, sodium acetate / methanol / 0.67 h / Heating

4: xylene / 0.83 h / 150 °C

5: sodium hydroxide / ethanol; H₂O / 7.25 h / Heating

6: 84 percent / H₂, (1S)-(+)-10-camphorsulfonic acid / palladium hydroxide on carbon / ethyl acetate / 22.5 h

7: 85 percent / N-ethyldiisopropylamine / 4-dimethylaminopyridine / CH₂Cl₂ / 1.) 0 deg C, 40 min; 2.) rt,1.33 h

8: lithium diisopropylamide / hexane; tetrahydrofuran / 1.) 0 deg C, 50 min; 2.) rt, 50 min

9: 83 percent / n-BuLi / hexane; tetrahydrofuran / 1.1 h / Ambient temperature

10: pyridinium p-toluenesulfonate / dimethylformamide / 0.83 h / Ambient temperature

11: sodium hydride / dimethylformamide / 1.25 h

12: 99 percent / acetic acid; tetrahydrofuran; propan-2-ol / 8.5 h / Ambient temperature

13: 88 percent / dicyclohexylcarbodiimide, pyridine, trifluoroacetic acid, DMSO / benzene / 4.5 h / Ambient temperature

14: 61 percent / (1S)-(+)-10-camphorsulfonic acid / methanol; toluene / 3 h / Ambient temperature

15: 65 percent / ethanethiol, sodium hydride / dimethylformamide / 1 h / 150 °C

With pyridine; potassium hydroxide; sodium hydroxide; n-butyllithium; hydroxylamine hydrochloride; hydrogen; sodium acetate; pyridinium p-toluenesulfonate; sodium hydride; dimethyl sulfoxide; (+)-10-camphorsulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; ethanethiol; lithium diisopropyl amide; dmap; palladium dihydroxide; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; acetic acid; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol; toluene; xylene; benzene;
DOI:10.1016/S0040-4020(01)83440-2