5,7-Di-tert-butyl-2,2-dimethyl-3-phenyl-2,3-dihydro-benzofuran-3-yl-hydroperoxide

Base Information

Chemical Name:5,7-Di-tert-butyl-2,2-dimethyl-3-phenyl-2,3-dihydro-benzofuran-3-yl-hydroperoxide
CAS No.:102520-05-8
Molecular Formula:C₂₄H₃₂O₃
Molecular Weight:368.516
Hs Code.:

Synonyms:5,7-Di-tert-butyl-2,2-dimethyl-3-phenyl-2,3-dihydro-benzofuran-3-yl-hydroperoxide

Suppliers and Price of 5,7-Di-tert-butyl-2,2-dimethyl-3-phenyl-2,3-dihydro-benzofuran-3-yl-hydroperoxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5,7-Di-tert-butyl-2,2-dimethyl-3-phenyl-2,3-dihydro-benzofuran-3-yl-hydroperoxide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5,7-Di-tert-butyl-2,2-dimethyl-3-phenyl-2,3-dihydro-benzofuran-3-yl-hydroperoxide

There total 4 articles about 5,7-Di-tert-butyl-2,2-dimethyl-3-phenyl-2,3-dihydro-benzofuran-3-yl-hydroperoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 102520-02-5
2,4-Di-tert-butyl-6-(2-methyl-1-phenyl-propenyl)-phenol

: 102520-05-8
5,7-Di-tert-butyl-2,2-dimethyl-3-phenyl-2,3-dihydro-benzofuran-3-yl-hydroperoxide

: 2,6-Di-tert-butyl-2-hydroxy-4-(2-methyl-1-phenyl-propenyl)-7-oxa-bicyclo[4.1.0]hept-4-en-3-one

: 102520-13-8
3,5-Di-tert-butyl-5-hydroxy-1-(2-methyl-1-phenyl-propenyl)-7-oxa-bicyclo[4.1.0]hept-3-en-2-one

Guidance literature:: With potassium tert-butylate; oxygen; In hexane; tert-butyl alcohol; for 9h; Ambient temperature;
DOI:10.1021/jo00362a018

Reference yield: 5.0%

: 102520-02-5
2,4-Di-tert-butyl-6-(2-methyl-1-phenyl-propenyl)-phenol

: 24242-58-8
(3,5-di-tert-butyl-2-hydroxyphenyl)(phenyl)methanone

: 102520-05-8
5,7-Di-tert-butyl-2,2-dimethyl-3-phenyl-2,3-dihydro-benzofuran-3-yl-hydroperoxide

Guidance literature:: With Co(Salpr); oxygen; In dichloromethane; for 30h; Ambient temperature;
DOI:10.1021/jo00362a018

Reference yield:

: 24242-58-8
(3,5-di-tert-butyl-2-hydroxyphenyl)(phenyl)methanone

: 102520-05-8
5,7-Di-tert-butyl-2,2-dimethyl-3-phenyl-2,3-dihydro-benzofuran-3-yl-hydroperoxide

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / 2.5 h / Heating

2: CH₃COOH / 0.17 h / Heating

3: 78 percent / Co(Salpr), O₂ / CH₂Cl₂ / 30 h / Ambient temperature

With Co(Salpr); oxygen; acetic acid; In diethyl ether; dichloromethane;
DOI:10.1021/jo00362a018