2-(chloromethyl)-6-[[3-(chloromethyl)-2-hydroxy-5-methyl-phenyl]methyl]-4-methylphenol

Base Information

• Chemical Name: 2-(chloromethyl)-6-[[3-(chloromethyl)-2-hydroxy-5-methyl-phenyl]methyl]-4-methylphenol
• CAS No.: 252062-98-9
• Molecular Formula: C₁₇H₁₈Cl₂O₂
• Molecular Weight: 325.235

Synonyms:2-(chloromethyl)-6-[[3-(chloromethyl)-2-hydroxy-5-methyl-phenyl]methyl]-4-methylphenol

Chemical Property of 2-(chloromethyl)-6-[[3-(chloromethyl)-2-hydroxy-5-methyl-phenyl]methyl]-4-methylphenol

Chemical Property:

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Technology Process of 2-(chloromethyl)-6-[[3-(chloromethyl)-2-hydroxy-5-methyl-phenyl]methyl]-4-methylphenol

There total 1 articles about 2-(chloromethyl)-6-[[3-(chloromethyl)-2-hydroxy-5-methyl-phenyl]methyl]-4-methylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-(3-hydroxymethyl-2-hydroxy-5-methylbenzyl)-6-hydroxymethyl-4-methylphenol (22247-58-1) → 2-(chloromethyl)-6-[[3-(chloromethyl)-2-hydroxy-5-methyl-phenyl]methyl]-4-methylphenol (252062-98-9)

Guidance literature:

With thionyl chloride; In benzene; at 20 ℃; for 5h;

DOI:10.1002/jhet.5570370113

Reference yield: 67.0%

2-(chloromethyl)-6-[[3-(chloromethyl)-2-hydroxy-5-methyl-phenyl]methyl]-4-methylphenol (252062-98-9) + N-methylaniline (100-61-8) → C31H34N2O2 (1422766-56-0)

Guidance literature:

With sodium hydrogencarbonate; In tetrahydrofuran; for 12h; Reflux; Inert atmosphere; Schlenk technique;

DOI:10.1039/c2dt32520a

Reference yield: 21.0%

2-(chloromethyl)-6-[[3-(chloromethyl)-2-hydroxy-5-methyl-phenyl]methyl]-4-methylphenol (252062-98-9) + (S)-2-((S)-2-Amino-3-phenyl-propionylamino)-3-[(S)-2-((S)-2-amino-3-phenyl-propionylamino)-2-methoxycarbonyl-ethyldisulfanyl]-propionic acid methyl ester; compound with GENERIC INORGANIC NEUTRAL COMPONENT → C60H66N4O10S2

Guidance literature:

With sodium carbonate; In N,N-dimethyl-formamide; at 30 ℃; for 18h;

DOI:10.1021/jo000738z

upstream raw materials:

2-(3-hydroxymethyl-2-hydroxy-5-methylbenzyl)-6-hydroxymethyl-4-methylphenol

Downstream raw materials:

bis-[2-hydroxy-3-(2-hydroxy-3,5-dimethyl-benzyl)-5-methyl-phenyl]-methane

bis-[2-acetoxy-3-(2-acetoxy-3,5-dimethyl-benzyl)-5-methyl-phenyl]-methane

C₃₁H₃₄N₂O₂

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